1-(6-Chloro-1-methyl-1H-imidazo-[4,5-c]pyridin-4-yl)-3-(2-chlorophenyl)-urea

被引：0
|
作者：
Devaru, Venkatesh B. [1 ]
Vinduvahini, M. [2 ]
Madaiah, M. [3 ]
Revanasiddappa, H. D. [3 ]
Devarajegowda, H. C. [4 ]
机构：
[1] LVD Coll, PG Dept Phys, Raichur 584103, Karnataka, India
[2] Sri D Devaraja Urs Govt First Grade Coll, Dept Phys, Mysore 571105, Karnataka, India
[3] Univ Mysore, Dept Studies Chem, Mysore 570006, Karnataka, India
[4] Univ Mysore, Yuvarajas Coll Constituent Coll, Dept Phys, Mysore 570005, Karnataka, India
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2014年 / 70卷
关键词：
data-to-parameter ratio = 12.9; mean σ(C-C) = 0.004 Å; R factor = 0.039; single-crystal X-ray study; T = 293 K; wR factor = 0.112;
D O I：
10.1107/S1600536814000695
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, C14H11Cl2N5O, the plane of the 1H-imidazo[4,5-c] pyridine ring system [r.m.s. deviation = 0.087 (19) angstrom] makes a dihedral angle of 4.87 (10)degrees with the terminal phenyl ring. An intramolecular N-H center dot center dot center dot N hydrogen bond stabilizes the molecular conformation. In the crystal, N-H center dot center dot center dot O hydrogen bonds link the molecules into inversion dimers. These dimers are connected by pi-pi interactions between imidazole rings [shortest centroid-centroid distance = 3.4443 (14) angstrom].
引用
收藏
页码：0155 / +
页数：8
相关论文
共 50 条
  • [1] N-(6-Chloro-1-methyl-1H-imidazo-[4,5-c]pyridin-4-yl)benzenesulfonamide
    Devaru, Venkatesh B.
    Katagi, K. S.
    Kotresh, O.
    Arunkashi, H. K.
    Devarajegowda, H. C.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : O445 - +
  • [2] Anti-oxidant activity of 1-(1H-imidazo[4,5-c]pyridin-4-yl)ethenone, a Maillard reaction product derived from fructose and histidine
    Zhao, Kangyu
    Long, Xin
    Li, Junle
    Wang, Ying
    Lan, Ping
    Wang, Yong
    JOURNAL OF THE SCIENCE OF FOOD AND AGRICULTURE, 2024, 104 (15) : 9548 - 9558
  • [3] 1-[6-Chloro-4-(2-chlorophenyl)-2-methyl-3-quinolyl]ethanone
    Preeti, B.
    Sarveswari, S.
    Vijayakumar, V.
    Tan, Kang Wai
    Tiekink, Edward R. T.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2010, 66 : O2002 - U1070
  • [4] 1-(8-Chloro-3-methyl-1H-pyrazolo[4,3-c]cinnolin-1-yl)-2-(2-chlorophenyl)ethanone
    Bawa, Sandhya
    Tonk, Rajiv K.
    Chawla, Gita
    Kumar, Suresh
    Afzal, Obaid
    MOLBANK, 2011, (04)
  • [5] 3-[(1-Isobutyl-1H-imidazo[4,5-c]quinolin-4-yl)amino]benzoic acid
    Fun, Hoong-Kun
    Shahani, Tara
    Dinesh
    Kayarmar, Reshma
    Nagaraja, G. K.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O2150 - U1553
  • [6] 1-(Prop-2-en-1-yl)-3-{[3-(pyridin-4-yl)-4,5-dihydroisoxazol-5-yl]methyl}-1H-anthra[1,2-d]imidazole-2,6,11(3H)-trione
    Afrakssou, Zahra
    Rodia, Youssef Kandri
    Capet, Frederic
    Essassi, El Mokhtar
    Rolando, Christian
    El Ammari, Lahcen
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O945 - +
  • [7] (8-Chloro-3-methyl-1H-pyrazolo[4,3-c]cinnolin-1-yl) (pyridin-4-yl)methanone
    Bawa, Sandhya
    Kumar, Rajiv
    Chawla, Gita
    Kumar, Suresh
    Mishra, Ravinesh
    MOLBANK, 2010, (02) : 1 - 3
  • [8] 1-(2-chlorophenyl)-3-[(phenyl)(4-tolylimino)methyl]thiourea
    Xing, Zhi-Yong
    Zhao, Hai-Tao
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O2268 - O2269
  • [9] SYNTHESIS OF 4-METHYL-1H-IMIDAZO[4,5-C]QUINOLINE
    GLUSHKOV, RG
    DAVIDOVA, NK
    MARCHENKO, NB
    KHIMIYA GETEROTSIKLICHESKIKH SOEDINENII, 1989, (02): : 231 - 232
  • [10] 1-(4-Chlorophenyl)-3-(morpholin-4-yl)urea
    Li, Yu-Feng
    Jiang, Jin-He
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O1219 - +
12345