LIQUID-CHROMATOGRAPHY MASS-SPECTROMETRY STUDIES OF 9-FLUORENYLMETHYL CHLOROFORMATE DERIVATIVES OF POLYAMINES

被引：5

作者：

LU, Z ^{[1
]}

VEENING, H ^{[1
]}

COUTANT, JE ^{[1
]}

机构：

[1] MERRELL DOW RES INST,CINCINNATI,OH 45215

来源：

JOURNAL OF CHROMATOGRAPHY | 1991年 / 540卷 / 1-2期

关键词：

D O I：

10.1016/S0021-9673(01)88809-9

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Liquid chromatography-mass spectrometry experiments were carried out to elucidate the structure of the carbamate derivatives formed when polyamines, such as ethylenediamine and putrescine, react with the precolumn fluorophore forming reagent, 9-fluorenylmethyl chloroformate. It has been shown that both primary amine functionalities derivatize with the reagent for polyamines.

引用

页码：199 / 206

页数：8

共 6 条

[1] HIGH-SENSITIVITY AMINO-ACID ANALYSIS BY DERIVATIZATION WITH ORTHO-PHTHALADEHYDE AND 9-FLUORENYLMETHYL CHLOROFORMATE USING FLUORESCENCE DETECTION - APPLICATIONS IN PROTEIN-STRUCTURE DETERMINATION
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CARDIN, AD
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[2] HIGH-RESOLUTION REVERSED-PHASE LIQUID-CHROMATOGRAPHY SYSTEM FOR THE ANALYSIS OF COMPLEX SOLUTIONS OF PRIMARY AND SECONDARY AMINO-ACIDS
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LAGERKVIST, S
[J]. ANALYTICAL CHEMISTRY, 1986, 58 (08) : 1638 - 1643
[3] SEPARATION OF AMINO-ACID ENANTIOMERS AND CHIRAL AMINES USING PRECOLUMN DERIVATIZATION WITH (+)-1-(9-FLUORENYL)ETHYL CHLOROFORMATE AND REVERSED-PHASE LIQUID-CHROMATOGRAPHY
EINARSSON, S
JOSEFSSON, B
MOLLER, P
SANCHEZ, D
[J]. ANALYTICAL CHEMISTRY, 1987, 59 (08) : 1191 - 1195
[4] DETERMINATION OF AMINO-ACIDS WITH 9-FLUORENYLMETHYL CHLOROFORMATE AND REVERSED-PHASE HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY
EINARSSON, S
JOSEFSSON, B
LAGERKVIST, S
[J]. JOURNAL OF CHROMATOGRAPHY, 1983, 282 (DEC): : 609 - 618
[5] HPLC OF 9-FLUORENYLMETHYLCHLOROFORMATE-POLYAMINE DERIVATIVES WITH FLUORESCENCE DETECTION
PRICE, JR
METZ, PA
VEENING, H
[J]. CHROMATOGRAPHIA, 1987, 24 : 795 - 799
[6] Yun Z, 1987, Biomed Chromatogr, V2, P173, DOI 10.1002/bmc.1130020410

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