Determination of polycyclic aromatic hydrocarbons in soil by ultra performance liquid chromatography

被引:0
作者
Chen Hao [1 ]
Liu Ying [1 ]
Liu Hailing [1 ]
Yuan Yuan [1 ]
Mao Qianfen [1 ]
机构
[1] Tongji Univ, Coll Environm Sci & Engn, State Key Lab Pollut Control & Resource Reuse, Shanghai 200092, Peoples R China
关键词
ultra performance liquid chromatography (UPLC); high performance liquid chromatography (HPLC); polycyclic aromatic hydrocarbons (PAHs); soil;
D O I
暂无
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
An analytical method based on ultra performance liquid chromatography (UPLC) coupled with a photodiode array (PDA) detector has been developed for the simultaneous determination of 16 polycyclic aromatic hydrocarbons (PAHs). The comparison of UPLC and the conventional high performance liquid chromatography (HPLC) has been carried out. The major advantages of UPLC over HPLC include the faster analysis speed, considerably increased sensitivity and significantly improved detection limit. By UPLC, the whole analytical process can be performed in 13.5 min and the limits of detection for the 16 PAHs were between 2 pg and 20 pg.
引用
收藏
页码:769 / 771
页数:3
相关论文
共 3 条
[1]   Effects-directed analysis of organic toxicants in wastewater effluent from Zagreb, Croatia [J].
Grung, Merete ;
Lichtenthaler, Rainer ;
Ahel, Marijan ;
Tollefsen, Knut-Erik ;
Langford, Katherine ;
Thomas, Kevin V. .
CHEMOSPHERE, 2007, 67 (01) :108-120
[2]   Validation (in-house and collaborative) of a method based on liquid chromatography for the quantitation of 15 European-priority polycyclic aromatic hydrocarbons in smoke flavourings: HPLC-method validation for 15 EU priority PAH in smoke condensates [J].
Simon, Rupert ;
Palme, Sonja ;
Anklam, Elke .
FOOD CHEMISTRY, 2007, 104 (02) :876-887
[3]   Analysis of polynuclear aromatic hydrocarbons in heavy products derived from coal and petroleum by high performance liquid chromatography [J].
Zhang, Changming ;
Zhang, Xiaohang ;
Yang, Jianli ;
Liu, Zhenyu .
JOURNAL OF CHROMATOGRAPHY A, 2007, 1167 (02) :171-177