DETERMINATION OF PHOSPHORUS IN COPPER-PHOSPHORUS ALLOYS, BY GLC TECHNIQUE

被引:1
|
作者
KONTOYANNAKOS, J
MARKANTONATOU, C
机构
[1] Inorganic and Analytical Chemistry Laboratories, National Technical University of Athens, Athens
关键词
Alloys; copper; Chromatography; gas-liquid; Phosphorus;
D O I
10.1007/BF02411364
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
A simple, sensitive, accurate and rapid gas chromatographic method for the quantitative determination of phosphorus in copper-phosphorus alloys is described. The method is based on the chlorination of the sample with carbon tetrachloride in a sealed glass capsule at 550°C. The volatile products are introduced into the gas chromatograph after crushing the capsule in a special device. The method is very quick (ca. 20 min), involves simple manipulations and the error is about ±0.5%. © 1979 Friedr. Vieweg & Sohn Verlagsgesellschaft mbH.
引用
收藏
页码:212 / 214
页数:3
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