INVESTIGATION OF PHASE-SENSITIVE C-13-DETECTED C-13-H-1 SHIFT CORRELATION SEQUENCES WITH PARTIAL AND FULL H-1-H-1 DECOUPLING AND PARTIAL SPECTRAL EDITING

被引:6
作者
CARPENTER, KA [1 ]
REYNOLDS, WF [1 ]
机构
[1] UNIV TORONTO,DEPT CHEM,TORONTO M5S 1A1,ONTARIO,CANADA
关键词
C-13-DETECTED C-13-H-1 SHIFT CORRELATION SEQUENCE; PHASE-SENSITIVE MODE; PARTIAL AND FULL H-1-H-1 DECOUPLING; PARTIAL SPECTRAL EDITING;
D O I
10.1002/mrc.1260300404
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Several different versions of the C-13-detected C-13-H-1 shift correlation sequence in phase sensitive mode with partial and full H-1-H-1 decoupling are described and evaluated. As expected, they show sensitivity advantages over their absolute value analogues. Further, it is possible partially to edit the 2D spectra since CH2 peaks are inverted relative to CH and CH3 peaks.
引用
收藏
页码:287 / 294
页数:8
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