GAS PHASE ANALYTICAL SEPARATION AND STRUCTURAL STUDY OF CERAMIDES

被引：23

作者：

CASPARRI.G

HORNING, EC

HORNING, MG

机构：

[1] Institute for Lipid Research, Baylor University College of Medicine, Houston

来源：

CHEMISTRY AND PHYSICS OF LIPIDS | 1969年 / 3卷 / 01期

关键词：

D O I：

10.1016/0009-3084(69)90024-3

中图分类号：

Q5 [生物化学]; Q7 [分子生物学];

学科分类号：

071010 ; 081704 ;

摘要：

Ceramides may be subjected to direct separation and structural study by gas phase analytical methods. Suitable derivatives may be prepared by reaction with silylating reagents (leading to trimethylsilyl ether derivatives), and separations may be carried out with 1% SE-30 columns by temperature programming at 2°/min to 340-350°C. The structure of individual ceramides is indicated by their mass spectra; both the acyl group and the sphingosine base moiety can be recognized in this way. © 1969.

引用

页码：1 / +

页数：1

共 8 条

[1]

CHAMBAZ EM, 1967, ANAL LETT, V1, P201

[2] CHEMISTRY AND METABOLISM OF SPHINGOLIPIDS . 3-OXO DERIVATIVES OF N-ACETYLSPHINGOSINE AND N-ACETYLDIHYDROSPHINGOSINE [J].