DETERMINATION OF SELECTED CARBOXYLIC-ACIDS AND ALCOHOLS IN GROUNDWATER BY GC-MS

被引:11
作者
BEIHOFFER, J
FERGUSON, C
机构
[1] Natl Enforcement Investigation Cent, Denver, CO
关键词
D O I
10.1093/chromsci/32.3.102
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
A simple, rapid, and specific method is presented for the determination of selected carboxylic acids and alcohols in water samples by gas chromatography-mass spectrometry (GC-MS). Water samples are injected directly onto a DB-FFAP column (J&W Scientific; Folsom, CA), which has an acidified polyethylene glycol phase. Compounds analyzed include aliphatic carboxylic acids, aromatic carboxylic acids, aliphatic alcohols, and phenols. The instrument response is linear over 2 orders of magnitude for alcohols and 3 orders of magnitude for carboxylic acids, with a detection limit of less than 10 mg/L for most compounds.
引用
收藏
页码:102 / 106
页数:5
相关论文
共 20 条
[1]   DETERMINATION OF CARBOXYLIC-ACIDS BY LIQUID-CHROMATOGRAPHY AFTER PHASE-TRANSFER-CATALYZED FLUOROGENIC LABELING [J].
ALLENMARK, S ;
CHELMINSKABERTILSSON, M .
JOURNAL OF CHROMATOGRAPHY, 1988, 456 (02) :410-416
[2]  
CAREL AB, 1988, LAB PRACT, V37, P95
[3]   GAS-CHROMATOGRAPHIC MASS-SPECTROMETRIC AND GAS-CHROMATOGRAPHIC FOURIER-TRANSFORM INFRARED-ANALYSIS OF ORGANIC-ACIDS - PRELIMINARY DATA [J].
CARUSO, U ;
ROMANO, C ;
RAVERDINO, V .
BIOMEDICAL AND ENVIRONMENTAL MASS SPECTROMETRY, 1988, 16 (1-12) :285-288
[4]  
DANESHVAR MI, 1988, J CHROMATOGR-BIOMED, V77, P4
[5]   A LIQUID-CHROMATOGRAPHY SYSTEM FOR MEASUREMENT OF ORGANIC-ACIDS IN PRECIPITATION [J].
ELBERT, W ;
HAHN, J ;
LERCH, M .
INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY, 1989, 35 (03) :149-159
[6]  
GROSJEAN D, 1989, J LIQ CHROMATOGR, V12, P3007
[7]  
HAGINAKA J, 1988, J CHROMATOGR, V447, P373, DOI 10.1016/0021-9673(88)90047-7
[8]   THE DETECTION OF ORGANIC-ACIDS IN A NON-OXIDATION MODE USING AN AMPEROMETRIC DETECTOR [J].
HAVNER, G ;
PANNELL, DK ;
TARTER, JG .
JOURNAL OF LIQUID CHROMATOGRAPHY, 1989, 12 (03) :299-305
[9]   SIMULTANEOUS GAS-CHROMATOGRAPHY OF VOLATILE AND NONVOLATILE CARBOXYLIC-ACIDS AS TERT-BUTYLDIMETHYLSILYL DERIVATIVES [J].
KIM, KR ;
HAHN, MK ;
ZLATKIS, A ;
HORNING, EC ;
MIDDLEDITCH, BS .
JOURNAL OF CHROMATOGRAPHY, 1989, 468 :289-301
[10]  
KOSSON DS, 1984, ENVIRON PROG, V3, P176