(3E,5E)-1-AllyI-3,5-bis(4-methoxybenzylidene)piperidin-4-one

被引:8
作者
Almansour, Abdulrahman I. [1 ]
Kumar, Raju Suresh [1 ]
Arumugam, Natarajan [1 ]
Vishnupriya, R. [2 ]
Suresh, J. [2 ]
机构
[1] King Saud Univ, Dept Chem, Coll Sci, Riyadh 11451, Saudi Arabia
[2] Madura Coll, Dept Phys, Madurai 625011, Tamil Nadu, India
关键词
D O I
10.1107/S1600536813015195
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The piperidine ring in the title compound, C24H25NO3, adopts an envelope conformation with the N atom being the flap atom, and each C=C double bond exhibits an E conformation. In the crystal, C-H center dot center dot center dot O hydrogen bonds link the molecules, forming supramolecular layers that stack along the a axis.
引用
收藏
页码:O1071 / +
页数:8
相关论文
共 10 条
[1]  
Bruker, 2004, APEX2 SAINT
[2]   GENERAL DEFINITION OF RING PUCKERING COORDINATES [J].
CREMER, D ;
POPLE, JA .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1975, 97 (06) :1354-1358
[3]   Conformational and quantitative structure-activity relationship study of cytotoxic 2-arylidenebenzocycloalkanones [J].
Dimmock, JR ;
Kandepu, NM ;
Nazarali, AJ ;
Kowalchuk, TP ;
Motaganahalli, N ;
Quail, JW ;
Mykytiuk, PA ;
Audette, GF ;
Prasad, L ;
Perjési, P ;
Allen, TM ;
Santos, CL ;
Szydlowski, J ;
De Clercq, E ;
Balzarini, J .
JOURNAL OF MEDICINAL CHEMISTRY, 1999, 42 (08) :1358-1366
[4]  
Dimmock JR, 1999, CURR MED CHEM, V6, P1125
[5]   ISOLATION AND CHARACTERIZATION OF A 1-PYRIDINE FUNGAL ALKALOID [J].
GUENGERICH, FP ;
DIMARI, SJ ;
BROQUIST, HP .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1973, 95 (06) :2055-2056
[6]   Streptazones A, B1, B2, C, and D:: New piperidine alkaloids from streptomycetes [J].
Puder, C ;
Krastel, P ;
Zeeck, A .
JOURNAL OF NATURAL PRODUCTS, 2000, 63 (09) :1258-1260
[7]  
Sheldrick G.M., 1996, SADABS VERSION 2008
[8]   A short history of SHELX [J].
Sheldrick, George M. .
ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122
[9]   Structure validation in chemical crystallography [J].
Spek, Anthony L. .
ACTA CRYSTALLOGRAPHICA SECTION D-STRUCTURAL BIOLOGY, 2009, 65 :148-155
[10]   (R)-3,5-Bis[(E)-benzylidene]-1-(1-phenylethyl)piperidin-4-one, 3,5-bis[(E)-4-chlorobenzylidene]-1-[(R)-1-phenylethyl]piperidin-4-one and 3,5-bis[(E)-2-chlorobenzylidene]-1-[(R)-1-phenylethyl]piperidin-4-one [J].
Suresh, J. ;
Kumar, R. Suresh ;
Perumal, S. ;
Natarajan, S. .
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2007, 63 (05) :O315-O318