SEPARATION AND ISOLATION OF VOLATILE ORGANIC-COMPOUNDS USING VACUUM DISTILLATION WITH GC/MS DETERMINATION

被引：26
|
作者：
HIATT, MH [1 ]
YOUNGMAN, DR [1 ]
DONNELLY, JR [1 ]
机构：
[1] LOCKHEED ENVIRONM SYST & TECHNOL CO,LAS VEGAS,NV 89119
来源：
ANALYTICAL CHEMISTRY | 1994年 / 66卷 / 06期
关键词：
D O I：
10.1021/ac00078a023
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
Vacuum distillation of water, soil, oil, and fish samples is presented as an alternative technique for determining volatile organic compounds (VOCs). Analyses of samples containing VOCs and non-VOCs at 50 ppb concentrations were performed to evaluate method limitations. Analyte recoveries were found to relate closing with boiling point unless a compound's water solubility exceeded 5 g/L. Recovery, precision, and method detection limits for VOCs demonstrate this technology is appropriate for environmental samples.
引用
收藏
页码：905 / 908
页数：4
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