STRUCTURAL ELUCIDATION OF ACETOGENINS FROM ANNONACEAE BY FAST-ATOM-BOMBARDMENT MASS-SPECTROMETRY

被引:25
作者
LAPREVOTE, O [1 ]
DAS, BC [1 ]
机构
[1] CNRS,INST CHIM SUBSTANCES NAT,F-91198 GIF SUR YVETTE,FRANCE
关键词
D O I
10.1016/S0040-4020(01)85568-X
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
The Annonaceous acetogenins form complexes with lithium in a liquid matrix. Fast atom bombardment (FAB) combined with linked scan (B/E) mass spectrometry of various lithium cationized acetogenins was used to analyze the collision-induced dissociations of these complexes. Characteristic fingerprints of the different structural types investigated have been obtained, allowing their unambiguous structural identification.
引用
收藏
页码:8479 / 8490
页数:12
相关论文
共 41 条
[21]   INVESTIGATIONS OF GAS-PHASE LITHIUM-PEPTIDE ADDUCTS - TANDEM MASS-SPECTROMETRY AND SEMIEMPIRICAL STUDIES [J].
LEARY, JA ;
ZHOU, ZG ;
OGDEN, SA ;
WILLIAMS, TD .
JOURNAL OF THE AMERICAN SOCIETY FOR MASS SPECTROMETRY, 1990, 1 (06) :473-480
[22]   COLLISION-INDUCED DISSOCIATION MASS-ANALYSED ION KINETIC-ENERGY (CID MIKE) ANALYSIS OF IONS GENERATED BY FAST ATOM BOMBARDMENT OF ISOMERIC BILE-SALTS [J].
LIEHR, JG ;
KINGSTON, EE ;
BEYNON, JH .
BIOMEDICAL MASS SPECTROMETRY, 1985, 12 (03) :95-99
[23]   COLLISIONAL ACTIVATION SPECTRA OF LI+ AND NA+ CATIONIZED DIELS-ALDER ADDUCTS OF SUBSTITUTED PARA-BENZOQUINONES AND GLUCOFURANODIENES [J].
MADHUSUDANAN, KP ;
DHAMI, TS ;
SURYAWANSHI, SN ;
BHAKUNI, DS .
ORGANIC MASS SPECTROMETRY, 1992, 27 (07) :837-839
[24]   HIGH-ENERGY COLLISION-INDUCED DISSOCIATION OF ALKALI-METAL ION ADDUCTS OF CROWN ETHERS AND ACYCLIC ANALOGS [J].
MALEKNIA, S ;
BRODBELT, J .
RAPID COMMUNICATIONS IN MASS SPECTROMETRY, 1992, 6 (06) :376-381
[25]   FAST ATOM BOMBARDMENT-TANDEM MASS-SPECTROMETRY STUDIES OF ORGANO-ALKALI METAL-IONS OF SMALL PEPTIDES [J].
MALLIS, LM ;
RUSSELL, DH .
ANALYTICAL CHEMISTRY, 1986, 58 (06) :1076-1080
[26]   SOME GENERAL-ASPECTS OF THE CHEMISTRY OF ORGANO-ALKALI METAL-IONS - AN OVERVIEW OF RECENT WORK [J].
MALLIS, LM ;
RUSSELL, DH .
INTERNATIONAL JOURNAL OF MASS SPECTROMETRY AND ION PROCESSES, 1987, 78 :147-178
[27]  
MCLAFFERTY FW, 1983, TANDEM MASS SPECTROM
[28]  
PUZO G, 1980, ADV MASS SPECTROM A, V8, P1003
[29]   LINKED SCAN INVESTIGATION OF PEPTIDE DEGRADATION INITIATED BY LIQUID SECONDARY ION MASS-SPECTROMETRY [J].
RENNER, D ;
SPITELLER, G .
BIOMEDICAL AND ENVIRONMENTAL MASS SPECTROMETRY, 1988, 15 (02) :75-77
[30]   ACETOGENINS OF ANNONACEAE .21. 2 ACETOGENINS FROM ANNONA-MURICATA SEEDS [J].
ROBLOT, F ;
LAUGEL, T ;
LEBOEUF, M ;
CAVE, A ;
LAPREVOTE, O .
PHYTOCHEMISTRY, 1993, 34 (01) :281-285