5-(Prop-2-ynyl)-5H-dibenzo[b,f]azepine

被引：6

作者：

Yousuf, S. ^{[1
]}

Khan, M. ^{[1
]}

Fazal, S. ^{[1
]}

Butt, M. ^{[1
]}

Basha, F. Z. ^{[1
]}

机构：

[1] Univ Karachi, Int Ctr Chem & Biol Sci, HEJ Res Inst Chem, Karachi 75270, Pakistan

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷

关键词：

D O I：

10.1107/S1600536812007866

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The asymmetric unit of the title compound, C17H13N, contains two independent butterfly-shaped molecules. The seven-membered azepine rings both adopt a boat conformation. The dihedral angles between the benzene rings in the two molecules are 46.95 (11) and 52.21 (11)degrees.

引用

页码：O1101 / +

页数：9

共 15 条

[1]

ARYA VP, 1977, INDIAN J CHEM B, V15, P148

[2]

Balaure PC, 2009, REV ROUM CHIM, V54, P935

[3]

Bhatt PV, 2005, INDIAN J CHEM B, V44, P2082

[4]

Bruker, 2000, SAINT SADABS

[5] A new type of mixed anhydride and its applications to the synthesis of 7-substituted 8-chloro-5,5-dioxoimidazo[1,2-b][1,4,2]benzodithiazines with in vitro antitumor activity [J].

Brzozowski, Z ;

Saczewski, F .

JOURNAL OF MEDICINAL CHEMISTRY, 2002, 45 (02) :430-437

[6] A new industrial process for oxcarbazepine [J].

Fuenfschilling, PC ;

Zaugg, W ;

Beutler, U ;

Kaufmann, D ;

Lohse, O ;

Mutz, JP ;

Onken, U ;

Reber, JL ;

Shenton, D .

ORGANIC PROCESS RESEARCH & DEVELOPMENT, 2005, 9 (03) :272-277

[7] Role of Cocrystal and Solution Chemistry on the Formation and Stability of Cocrystals with Different Stoichiometry [J].

Jayasankar, Adivaraha ;

Reddy, L. Sreenivas ;

Bethune, Sarah J. ;

Rodriguez-Hornedo, Nair .

CRYSTAL GROWTH & DESIGN, 2009, 9 (02) :889-897

[8] CONTRA-THERMODYNAMIC TRANSESTERIFICATION OF CARBAMATES BY COUNTERATTACK STRATEGY - A VIABLE NON-PHOSGENE, NON-MIC ROUTE TO CARBAMATE PESTICIDES [J].

KULKARNI, GH ;

NAIK, RH ;

TANDEL, SK ;

RAJAPPA, S .

TETRAHEDRON, 1991, 47 (07) :1249-1256

[9] Synthesis and antioxidant properties of some novel 5H-dibenz[b,f]azepine derivatives in different in vitro model systems [J].

Kumar, H. Vijay ;

Naik, Nagaraja .

EUROPEAN JOURNAL OF MEDICINAL CHEMISTRY, 2010, 45 (01) :2-10

[10] 10-Methoxy-5H-dibenz[b,f]azepine [J].

Nagaraj, B ;

Yathirajan, HS ;

Lynch, DE .

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 :O1757-O1759

← 1 2 →