3-Carboxyquinolin-1-ium-2-carboxylate monohydrate

被引：3

作者：

Wang, Xing ^{[1
]}

Liu, Chun-Bo ^{[1
]}

Yan, Yong-Sheng ^{[1
]}

Wang, Shen-Tang ^{[1
]}

Zhang, Qing ^{[1
]}

机构：

[1] Jiangsu Univ, Sch Chem & Chem Engn, Zhenjiang 212013, Peoples R China

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷

关键词：

data-to-parameter ratio = 10.8; mean σ(C-C) = 0.002 Å; R factor = 0.036; single-crystal X-ray study; T = 153 K; wR factor = 0.101;

D O I：

10.1107/S1600536812006988

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The title compound, C 11H 7NO 4·H 2O, contains a 3-carb-oxy-quinolin-1-ium-2-carboxyl-ate (qda) zwitterion and one water mol-ecule. In the crystal, pairs of N - H⋯O hydrogen bonds link the mol-ecules into inversion dimers, and these dimers are further connected by O - H⋯O hydrogen bonds into a three-dimensional supra-molecular architecture. In addition, π-π inter-actions occur between pyridine and benzene rings from different qda ligands [centroid-centroid distance = 3.749 (1) Å] and the dihedral angles of the -CO 2H and -CO 2 groups to the quinoline system are 8.47 (3) and 88.16 (6)°, respectively.

引用

页码：O829 / U2910

页数：7

共 11 条

[1]

Brandenburg K., 1998, DIAMOND

[2] Crystal structure and characterization of manganese(II) carboxylates: 3D metal-organic frameworks [J].

Dobrzynska, D ;

Jerzykiewicz, LB ;

Jezierska, J ;

Duczmal, M .

CRYSTAL GROWTH & DESIGN, 2005, 5 (05) :1945-1951

[3] Synthesis, spectroscopy, and magnetic properties of FeII and CoII quinoline-2-carboxylates -: Crystal structure of trans-bis(quinoline-2-carboxylato)bis(propanol)iron(II) [J].

Dobrzynska, D ;

Duczmal, M ;

Jerzykiewicz, LB ;

Warchulska, J ;

Drabent, K .

EUROPEAN JOURNAL OF INORGANIC CHEMISTRY, 2004, (01) :110-117

[4] trans-Bis(methanol-κO)bis(quinoline-2carboxylato-κ2N,O)manganese(II) [J].

Dobrzynska, Danuta ;

Jerzykiewicz, Lucjan B. .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 :M1383-U338

[5] Poly[bis(μ2-quinoline-3-carboxylato-κ2N:O)zinc(II)] [J].

Hu, Sheng ;

Zhang, Shu-Hua ;

Zeng, Ming-Hua .

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 :M2565-U1148

[6] Crystal structure of bis(hydrogen 2,3-quinolinedicarboxylato)copper(II), Cu(C11H6NO4)2 [J].

Li, Xiao-Ling ;

Liu, Guang-Zhen .

ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2010, 225 (04) :761-762

[7] trans-diaquabis(quinoline-2-carboxylato-N,O)-nickel(II)-water-ethanol (1/2/2) [J].

Odoko, M ;

Muranishi, Y ;

Okabe, N .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2001, 57 :m267-m269

[8]

Rigaku Corporation, 2007, CRYSTALCLEAR

[9] A short history of SHELX [J].

Sheldrick, George M. .

ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122

[10] A series of Cd(II) complexes with π-π stacking and hydrogen bonding interactions: Structural diversities by varying the ligands [J].

Wang, Xiuli ;

Zhang, Jinxia ;

Liu, Guocheng ;

Lin, Hongyan .

JOURNAL OF SOLID STATE CHEMISTRY, 2011, 184 (02) :280-288

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