N-(3,5-Dimethylphenyl)-4-nitrobenzene-sulfonamide

被引：0

作者：

Chaithanya, U. ^{[1
]}

Foro, Sabine ^{[2
]}

Gowda, B. Thimme ^{[1
]}

机构：

[1] Mangalore Univ, Dept Chem, Mangalore 574199, India

[2] Tech Univ Darmstadt, Inst Mat Sci, D-64287 Darmstadt, Germany

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷

关键词：

data-to-parameter ratio = 9.5; mean ω(C-C) = 0.006 Å; R factor = 0.039; single-crystal X-ray study; T = 293 K; wR factor = 0.074;

D O I：

10.1107/S1600536812047502

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

There are two independent molecules in the asymmetric unit of the title compound, C14H14N2O4S, in which the dihedral angles between the benzene rings are 56.22 (15) and 58.16 (14)degrees. In the crystal, N-H center dot center dot center dot Onitro hydrogen bonds link the molecules into zigzag chains running along the a-axis direction.

引用

页码：O3425 / +

页数：10

共 9 条

[1] Hydrogen bonding in sulfonamides [J].

Adsmond, DA ;

Grant, DJW .

JOURNAL OF PHARMACEUTICAL SCIENCES, 2001, 90 (12) :2058-2077

[2] N-(3,5-Dimethylphenyl)-2-nitrobenzene-sulfonamide [J].

Chaithanya, U. ;

Foro, Sabine ;

Gowda, B. Thimme .

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 :O2823-+

[3] ON ENANTIOMORPH-POLARITY ESTIMATION [J].

FLACK, HD .

ACTA CRYSTALLOGRAPHICA SECTION A, 1983, 39 (NOV) :876-881

[4]

GOWDA BT, 1994, Z NATURFORSCH A, V49, P695

[5]

Oxford Diffraction, 2009, CRYSALIS CCD CRYSALI

[6] 3-Acetyl-1-(2-methylphenyl) thiourea [J].

Shahwar, Durre ;

Tahir, M. Nawaz ;

Chohan, Muhammad Mansha ;

Ahmad, Naeem ;

Raza, M. Asam .

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 :O1160-+

[7] A short history of SHELX [J].

Sheldrick, George M. .

ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122

[8]

Shetty M, 2004, Z NATURFORSCH B, V59, P63

[9] Structure validation in chemical crystallography [J].

Spek, Anthony L. .

ACTA CRYSTALLOGRAPHICA SECTION D-STRUCTURAL BIOLOGY, 2009, 65 :148-155

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