An Efficient One-Pot Strategies for the Synthesis of [1,3] Oxazine Derivatives

被引：12
|
作者：
Sapkal, Suryakant B. [1 ]
Shelke, Kiran F. [1 ]
Shingate, Bapurao B. [1 ]
Shingare, Murlidhar S. [1 ]
机构：
[1] Dr Babasaheb Ambedkar Marathwada Univ, Dept Chem, Aurangabad 431004, MS, India
来源：
JOURNAL OF THE KOREAN CHEMICAL SOCIETY-DAEHAN HWAHAK HOE JEE | 2010年 / 54卷 / 04期
关键词：
1,3] Oxazine derivatives; One-pot strategies; Cyclocondensation; Ionic liquid; Grinding;
D O I：
10.5012/jkcs.2010.54.4.437
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Sodium hydrogen sulphate (NaHSO4), n-tetra butyl ammonium bromide (TBAB) as a phase transfer catalyst (PTC) in water, and 1-butyl-3-methyl imidazolium hydrogen sulphate [bmim] HSO4 as ionic liquid (IL) has been used as a mild reaction promoter for the cyclocondensation of formalin, beta-naphthol and aromatic amines to afford respective 2,3-dihydro-2phenyl-1H-naphtho-[1,2-e] [1,3] oxazine derivatives. The present protocols are greener, high yielding and involved the non-chromatographic isolation procedure.
引用
收藏
页码：437 / 442
页数：6
相关论文
共 50 条
  • [21] ONE-POT SYNTHESIS OF 5H-INDAZOLO-[3,2-b] BENZO[d]-1,3OXAZINE: TWO EFFICIENT PREPARATIVE METHODS
    Solano, Danielle M.
    Butler, Jeffrey D.
    Haddadin, Makhluf J.
    Kurth, Mark J.
    ORGANIC SYNTHESES, 2010, 87 : 339 - +
  • [22] A novel, one-pot synthesis of 2H-benz[e]-1,3-oxazine-2-thiones
    Yadav, LDS
    Saigal, S
    Pal, DR
    JOURNAL OF CHEMICAL RESEARCH-S, 1998, (06): : 307 - 307
  • [23] One-Pot Multicomponent Synthesis and Anticancer Activity of 1,3-Cyclopentathiazine and Pyrimidothiazine Derivatives
    R. A. Haggam
    H. Y. Moustafa
    M. G. Assy
    H. M. Abd El-Rahman
    Russian Journal of Organic Chemistry, 2020, 56 : 916 - 923
  • [24] One-Pot Multicomponent Synthesis and Anticancer Activity of 1,3-Cyclopentathiazine and Pyrimidothiazine Derivatives
    Haggam, R. A.
    Moustafa, H. Y.
    Assy, M. G.
    Abd El-Rahman, H. M.
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2020, 56 (05) : 916 - 923
  • [25] An efficient Biginelli one-pot synthesis of new naphthalene-condensed oxazine derivatives under microwave-assisted conditions
    Azizian, Javad
    Yadollahzadeh, Khadijeh
    Delbari, Akram Sadat
    Ghanbari, Mohammad Mehdi
    MONATSHEFTE FUR CHEMIE, 2012, 143 (10): : 1417 - 1420
  • [26] Efficient, One-Pot Synthesis of Pyrido[3,2-d]pyrimidine Derivatives
    Majumdar, K. C.
    Ponra, Sudipta
    Ghosh, Debankan
    SYNTHESIS-STUTTGART, 2011, (07): : 1132 - 1136
  • [27] An efficient Biginelli one-pot synthesis of new naphthalene-condensed oxazine derivatives under microwave-assisted conditions
    Javad Azizian
    Khadijeh Yadollahzadeh
    Akram Sadat Delbari
    Mohammad Mehdi Ghanbari
    Monatshefte für Chemie - Chemical Monthly, 2012, 143 : 1417 - 1420
  • [28] An Efficient One-Pot Synthesis of 1-Aminophosphonates
    Kaboudin, Babak
    Faghih, Samaneh
    Alavi, Sajedeh
    Naimi-jamal, Mohammad Reza
    Fattahi, Alireza
    SYNTHESIS-STUTTGART, 2023, 55 (01): : 121 - 130
  • [29] An Efficient One-Pot Synthesis of Dispiropyrrolidine Derivatives Through 1,3-Dipolar Cycloaddition Reactions Under Ultrasound Irradiation
    Liu, Hai
    Zou, Yi
    Hu, Yu
    Shi, Da-Qing
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 2011, 48 (04) : 877 - 881
  • [30] One-pot synthesis of imidazopyridine derivatives
    Parenty, Alexis D. C.
    Cronin, Leroy
    SYNTHESIS-STUTTGART, 2008, (09): : 1479 - 1485
12345