Crystal structure of (E)-1-(4-methoxyphenyl)ethanone O-dehydroabietyloxime

被引：0

作者：

Rao, Xiao-Ping ^{[1
]}

Cui, Yan-Jie ^{[1
]}

Zheng, Jian-Qiang ^{[1
]}

机构：

[1] Chinese Acad Forestry, Inst Chem Ind Forest Prod, Key Lab Biomass Energy & Mat, Natl Engn Lab Biomass Chem Utilizat,Key & Lab For, Nanjing 210042, Jiangsu, Peoples R China

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2014年 / 70卷

关键词：

crystal structure; oxime; dehydroabietic acid derivative; biological compounds;

D O I：

10.1107/S1600536814016882

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C29H37NO3 {systematic name: (E)-1-(4methoxyphenyl) ethanone O-[(1R, 4aS, 10aR)-7-isopropyl-1,4adimethyl-1,2,3,4,4a, 9,10,10a-octahydrophenanthrene-1-carbonyl] oxime}, a new derivative of dehydroabietic acid, the two cyclohexane rings exhibit a trans-ring junction and are in chair and half-chair conformations. The C=N double bond exhibits an E conformation.

引用

页码：O948 / +

页数：9

共 9 条

[1]

Cui YJ, 2013, LETT DRUG DES DISCOV, V10, P102

[2]

Enraf-Nonius, 1989, CAD 4 SOFTW

[3]

Harms K., 1995, XCAD4

[4] Cytotoxic effects and pro-apoptotic mechanism of TBIDOM, a novel dehydroabietylamine derivative, on human hepatocellular carcinoma SMMC-7721 cells [J].

Li, Fu ;

He, Ling ;

Song, Zhan-Qian ;

Yao, Jin-Cheng ;

Rao, Xiao-Ping ;

Li, Hai-Tao .

JOURNAL OF PHARMACY AND PHARMACOLOGY, 2008, 60 (02) :205-211

[5] A SEMI-EMPIRICAL METHOD OF ABSORPTION CORRECTION [J].

NORTH, ACT ;

PHILLIPS, DC ;

MATHEWS, FS .

ACTA CRYSTALLOGRAPHICA SECTION A-CRYSTAL PHYSICS DIFFRACTION THEORETICAL AND GENERAL CRYSTALLOGRAPHY, 1968, A 24 :351-&

[6] Dehydroabietic acid [J].

Rao, Xiao-Ping ;

Song, Zhan-Qian ;

Shang, Shi-Bin .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 :O2402-+

[7] Synthesis, Structure Analysis and Cytotoxicity Studies of Novel Unsymmetrically N,N′-Substituted Ureas from Dehydroabietic Acid [J].

Rao, Xiaoping ;

Song, Zhanqian ;

He, Ling ;

Jia, Weihong .

CHEMICAL & PHARMACEUTICAL BULLETIN, 2008, 56 (11) :1575-1578

[8] Gastroprotective and cytotoxic effect of dehydroabietic acid derivatives [J].

Sepúlveda, B ;

Astudillo, L ;

Rodríguez, JA ;

Yáñez, T ;

Theoduloz, C ;

Schmeda-Hirschmann, G .

PHARMACOLOGICAL RESEARCH, 2005, 52 (05) :429-437

[9] A short history of SHELX [J].

Sheldrick, George M. .

ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122

← 1 →