ONE-POT SYNTHESIS OF 1,5-BENZODIAZEPINE DERIVATIVES CATALYZED LEAD ACETATE UNDER SOLVENT FREE CONDITION

被引：0
|
作者：
Patil, Vishvanath D. [1 ]
Patil, Ketan P. [1 ]
Sutar, Nagesh R. [1 ]
Gidh, Prathamesh V. [1 ]
机构：
[1] CK Thakur ACS Coll New Panvel, Dept Chem, Organ Chem Res Lab, Raigad, Maharashtra, India
来源：
Heterocyclic Letters | 2016年 / 6卷 / 01期
关键词：
Lead acetate; o-phenylenediamine; ketones; 1,5-benzodiazepines; solvent free;
D O I：
暂无
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
A simple and efficeint method has been developed for synthesis of 1,5-benzdiazepines from o- phenylenediamine and substituted ketones in presence of a catalytic amount of Lead acetate at room temperature under solvent free condition. The remarkable selectivity under mild, neutral and, inexpensive catalystare attractive features.
引用
收藏
页码：61 / 69
页数：9
相关论文
共 50 条
  • [1] Molecular-iodine-catalyzed one-pot synthesis of 1,5-benzodiazepine derivatives under solvent-free conditions
    Chen, WY
    Lu, J
    SYNLETT, 2005, (08) : 1337 - 1339
  • [2] One pot solvent-free synthesis of 1,5-benzodiazepine derivatives
    Langade, M., 1600, Journal of Chemical and Pharmaceutical Research, 3/668 Malviya Nagar, Jaipur, Rajasthan, India (05):
  • [3] Organocatalyzed One-Pot Synthesis of Substituted 1,5-Benzodiazepine and Benzimidazole Derivatives
    Goswami, Papori
    Das, Babulal
    SYNTHETIC COMMUNICATIONS, 2010, 40 (11) : 1685 - 1693
  • [4] Sulfanilic acid catalyzed solvent-free synthesis of 1,5-benzodiazepine derivatives
    Jaiprakash N.Sangshetti
    Nagnnath D.Kokare
    Devanand B.Shinde
    Chinese Chemical Letters, 2007, (11) : 1305 - 1308
  • [5] A mild and efficient synthesis of 1,5-benzodiazepine derivatives catalyzed by acidic ionic liquid in solvent free condition
    Roy, Anupam
    Majee, Adinath
    Hajra, Alakananda
    JOURNAL OF THE INDIAN CHEMICAL SOCIETY, 2012, 89 (07) : 963 - 965
  • [6] Sulfanilic acid catalyzed solvent-free synthesis of 1,5-benzodiazepine derivatives
    Sangshetti, Jaiprakash N.
    Kokare, Nagnnath D.
    Shinde, Devanand B.
    CHINESE CHEMICAL LETTERS, 2007, 18 (11) : 1305 - 1308
  • [7] An Efficient One-Pot Synthesis of 1, 5-Benzodiazepine Derivatives Catalyzed by TBAB under Mild Conditions
    Baseer, Mohammad A.
    Khan, Asgar Jafar
    E-JOURNAL OF CHEMISTRY, 2012, 9 (01) : 407 - 414
  • [8] Highly efficient one-pot, three-component synthesis of 1,5-benzodiazepine derivatives
    Li, Xiao-Qing
    Wang, Lan-Zhi
    CHINESE CHEMICAL LETTERS, 2014, 25 (02) : 327 - 332
  • [9] Short oligo ethylene glycolic tailor-made ionic liquids as highly efficient and reusable catalyst for one-pot synthesis of 1,5-benzodiazepine derivatives under solvent free condition
    Jadhav, Arvind H.
    Chinnappan, Amutha
    Patil, Roopa H.
    Kostjuk, Sergei V.
    Kim, Hern
    CHEMICAL ENGINEERING JOURNAL, 2014, 240 : 228 - 234
  • [10] One-pot three-component reaction providing 1,5-benzodiazepine derivatives
    Murai, Kenichi
    Nakatani, Ryo
    Kita, Yasuyuki
    Fujioka, Hiromichi
    TETRAHEDRON, 2008, 64 (49) : 11034 - 11040
12345