A METHOD FOR THE DETERMINATION OF HISTAMINE IN WINE BY HPLC WITH PRECOLUMN DERIVATIZATION WITH PHENYLISOTHIOCYANATE

被引:20
作者
CALULL, M [1 ]
MARCE, RM [1 ]
FABREGAS, J [1 ]
BORRULL, F [1 ]
机构
[1] UNIV BARCELONA,DEPT QUIM,PCA IMPERIAL TARRACO 1,E-43005 TARRAGONA,SPAIN
关键词
COLUMN LIQUID CHROMATOGRAPHY; HISTAMINE IN WINE; PRECOLUMN DERIVATIZATION; SOLID PHASE EXTRACTION;
D O I
10.1007/BF02274560
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
A method for determining histamine in wine by precolumn derivatization with PITC (phenylisothiocyanate) with reversed-phase HPLC and UV detection is reported. Histamine can be determined together with the 24 amino acids within 40 min, or separately in a shorter time (less than 4 min) if a prior solid phase extraction clean-up is used.
引用
收藏
页码:133 / 136
页数:4
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