DuPont Zorbax C8 and Nucleosil CN columns were used to quantitatively and qualitatively determine Arquad 2C-75 additive in the rolling oils and the residual oils extracted from rolled aluminum products using an Indirect Photometric Chromatography (IPC) method. The most important finding is that the first negative peak is believed to be an indication of the presence of quaternary ammonium salts. The results obtained from the analyses of several commercial quaternary ammonium salts, amines and a normal paraffin oil in different solvent systems confirm this observation.