DRAMATIC INFLUENCE OF NITROGEN-HETEROCYCLES ON THE ACTIVITY OF LOW-VALENT TITANIUM REAGENT - AN IMPROVED ONE-POT SYNTHESIS OF PHENANTHRENES

被引：6
作者：
KADAM, SM [1 ]
NAYAK, SK [1 ]
BANERJI, A [1 ]
机构：
[1] BHABHA ATOM RES CTR,DIV BIOORGAN,BOMBAY 400085,INDIA
来源：
SYNTHETIC COMMUNICATIONS | 1995年 / 25卷 / 02期
关键词：
D O I：
10.1080/00397919508010799
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
A novel low-valent titanium (LVT) induced one-pot synthesis of phenanthrenes (25-38% yield) from ortho-alkoxy aromatic aldehydes/ketones was reported by us earlier. Activity of LVT complex could be modulated rationally by using catalytic amount of pyridine. Use of this LVT-pyridine reagent system improved the yields of phenanthrenes (3) by two folds.
引用
收藏
页码：135 / 142
页数：8
相关论文
共 50 条
[21]   Synthesis of quinazolines and imidazo[1,2-c]quinazolines with the aid of a low-valent titanium reagent [J].
Shi, DQ ;
Wang, JX ;
Shi, CL ;
Rong, LG ;
Zhuang, QY ;
Hu, HW .
SYNLETT, 2004, (06) :1098-1100
[22]   Transition metal-free one-pot synthesis of nitrogen-containing heterocycles [J].
Kumari, Simpal ;
Kishore, Dharma ;
Paliwal, Sarvesh ;
Chauhan, Rajani ;
Dwivedi, Jaya ;
Mishra, Aakanksha .
MOLECULAR DIVERSITY, 2016, 20 (01) :185-232
[23]   Transition metal-free one-pot synthesis of nitrogen-containing heterocycles [J].
Simpal Kumari ;
Dharma Kishore ;
Sarvesh Paliwal ;
Rajani Chauhan ;
Jaya Dwivedi ;
Aakanksha Mishra .
Molecular Diversity, 2016, 20 :185-232
[24]   An efficient one-step synthesis of 2-arylquinolin-4(1H)-ones with the aid of a low-valent titanium reagent [J].
Sun, Fang ;
Zhao, Xuan ;
Shi, Daqing .
TETRAHEDRON LETTERS, 2011, 52 (43) :5633-5635
[25]   An Efficient Synthesis of Pyrrolo[1,2-a]quinazolin-5(1H)-one Derivatives with the Aid of Low-Valent Titanium Reagent [J].
Zhao, Xuan ;
Shi, Da-Qing .
JOURNAL OF HETEROCYCLIC CHEMISTRY, 2011, 48 (03) :634-638
[26]   One-Pot Synthesis of Five and Six Membered N, O, S-Heterocycles Using a Ditribromide Reagent [J].
Yella, Ramesh ;
Patel, Bhisma K. .
JOURNAL OF COMBINATORIAL CHEMISTRY, 2010, 12 (05) :754-763
[27]   Highly Regioselective Synthesis of Polysubstituted Pyrroles through Three-Component Reaction Induced by Low-Valent Titanium Reagent [J].
Dou, Guolan ;
Shi, Chunling ;
Shi, Daqing .
JOURNAL OF COMBINATORIAL CHEMISTRY, 2008, 10 (06) :810-813
[28]   A facile synthesis of 1,2-dihydroquinazolin-4(3H)-ones with the aid of a low-valent titanium reagent [J].
Shi, DQ ;
Wang, JX ;
Rong, L ;
Zhuang, QY ;
Tu, SJ ;
Hu, HW .
JOURNAL OF CHEMICAL RESEARCH, 2003, (10) :671-673
[29]   One-Pot Synthesis of Alumina-Titanium Diboride Composite Powder at Low Temperature [J].
Liu, Xueyin ;
Bao, Ke ;
Chen, Junfeng ;
Jia, Quanli ;
Zhang, Shaowei .
MATERIALS, 2021, 14 (16)
[30]   One-Pot Synthesis of Magnesium Aminoclay-Titanium Dioxide Nanocomposites for Improved Photocatalytic Performance [J].
Bui, Vu K. H. ;
Park, Duckshin ;
Tran, Vinh V. ;
Lee, Go-Woon ;
Oh, Seo Yeong ;
Huh, Yun Suk ;
Lee, Young-Chul .
JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY, 2018, 18 (09) :6070-6074
12345