SYNTHESIS OF 3-ALKYL-5-POLYFLUOROALKYL-2-ISOXAZOLINES VIA 1,3-DIPOLAR CYCLOADDITION OF TRIMETHYLSILYL NITRONATES TO POLYFLUOROALKYLETHENES

被引:2
|
作者
CHEN, J [1 ]
HU, CM [1 ]
机构
[1] CHINESE ACAD SCI,SHANGHAI INST ORGAN CHEM,SHANGHAI 200032,PEOPLES R CHINA
关键词
SYNTHESIS; ALKYLPOLYFLUOROALKYLISOXAZOLINES; 1,3-DIPOLAR CYCLOADDITION; TRIMETHYLSILYL NITRONATES; POLYFLUOROALKYLETHENES;
D O I
10.1016/0022-1139(94)03142-M
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
Various 3-alkyl-5-polyfluoroalkyl-2-isoxazoline derivatives have been synthesized in moderate yield by the 1,3-dipolar cycloaddition reaction of nitroalkanes via their trimethylsilyl esters with polyfluoroalkylethenes.
引用
收藏
页码:43 / 46
页数:4
相关论文
共 50 条
  • [21] AN EFFICIENT AND CONVENIENT SYNTHESIS OF 4-POLYFLUOROALKYLATED PYRROLE-3-CARBOXYLATES THROUGH 1,3-DIPOLAR CYCLOADDITION REACTION OF POLYFLUORO-2-ALKYNOIC ACID-ESTERS WITH MUNCHNONES
    FUNABIKI, K
    ISHIHARA, T
    YAMANAKA, H
    JOURNAL OF FLUORINE CHEMISTRY, 1995, 71 (01) : 5 - 7
  • [22] Experimental and theoretical push-pull chemo- and regioselectivity in 1,3-dipolar cycloaddition reactions: The case of benzotriazepin-5-one with mesitylnitrile oxide
    Azzouzi, Saida
    Jala, Rachid
    El Messaoudi, Malika
    Domingo, Luis R.
    Esseffar, M'hamed
    Jose Aurell, M.
    JOURNAL OF PHYSICAL ORGANIC CHEMISTRY, 2007, 20 (04) : 245 - 254
  • [23] Synthesis and biological activity of potential antiviral compounds through 1,3-dipolar cycloadditions. Part 2: nitrones, nitrile oxides and imines, and other 1,3-dipoles
    Faita, Giuseppe
    Mella, Mariella
    Quadrelli, Paolo
    ARKIVOC, 2022, : 257 - 294
  • [24] Synthesis of spiro[indoline-3,3′-pyrrolizines] by 1,3-dipolar reactions between isatins, L-proline and electron-deficient alkenes
    Quiroga, Jairo
    Romo, Pablo
    Cobo, Justo
    Glidewell, Christopher
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2017, 73 : 1109 - +
  • [25] Synthesis and spectroscopic and structural characterization of spiro[inactime-3,3′-indolizine]s formed by 1,3-dipolar cycloadditions between isatins, pipecolic acid and an electron-deficient alkene
    Romo, Pablo E.
    Quiroga, Jairo
    Cobo, Justo
    Glidewell, Christopher
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2021, 77 : 496 - +
  • [26] Synthesis of (S, S)-1, 5-bis(4-alkyl-5-hydroxy-2-oxo-3-azapentyl)-1, 5-diazacyclooetane
    Shang, ZL
    Shang, ZC
    Yu, QS
    CHINESE CHEMICAL LETTERS, 2001, 12 (09) : 769 - 770
  • [27] Synthesis of highly substituted pyrrolidines via palladium catalysed formal [2+3] cycloaddition of 5-vinyloxazolidin-2-ones to activated alkenes
    Knight, JG
    Tchabanenko, K
    Stoker, PA
    Harwood, SJ
    TETRAHEDRON LETTERS, 2005, 46 (37) : 6261 - 6264
  • [28] One-pot synthesis of novel polysubstituted 1,1′-phenylene-bipyrrole via the double [3+2] cycloaddition reaction
    Liu, Huijun
    Ueta, Shoko
    Yagishita, Fumitoshi
    Nishiuchi, Masaki
    Kawamura, Yasuhiko
    TETRAHEDRON, 2015, 71 (22) : 3614 - 3618
  • [30] Synthesis of 3,3,5,5-tetrabenzyl-1,2,4-trithiol and 1,2-dis(1,3-arylpropan-2-yl)disulfane
    Feng, Fu
    Huang, Meng
    Duan, Zheng-Chao
    Hu, Wei-Bing
    CHINESE CHEMICAL LETTERS, 2013, 24 (10) : 909 - 911