(Z)-4-(3-Fluorophenyl)-1-(5-nitro-2-oxo-indolin-3-ylidene)thiosemicarbazide

被引：1
作者：
Pervez, Humayun [1 ]
Manzoor, Nazia [1 ]
Yaqub, Muhammad [1 ]
Tahir, M. Nawaz [2 ]
机构：
[1] Bahauddin Zakariya Univ, Dept Chem, Multan 60800, Pakistan
[2] Univ Sargodha, Dept Phys, Sargodha, Pakistan
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷
关键词：
data-to-parameter ratio = 16.5; mean σ(C-C) = 0.002 Å; R factor = 0.037; single-crystal X-ray study; T = 296 K; wR factor = 0.102;
D O I：
10.1107/S1600536812005053
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, C 15H 10FN 5O 3S, an intra-molecular N - H⋯N hydrogen bond generates an S(5) ring, whereas N - H⋯O and C - H⋯S interactions complete S(6) ring motifs. The dihedral angle between the isatin ring system and the fluoro-benzene ring is 5.96 (6)° and the complete molecule is close to planar (r.m.s. deviation for all the non-H atoms = 0.112 Å). In the crystal, molecules are linked by N - H⋯O hydrogen bonds to form C(8) chains along the [100] direction and C - H⋯O interactions are also observed.
引用
收藏
页码：O670 / U1865
页数：8
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