METHOD FOR THE ANALYSIS OF NON-ORTHO SUBSTITUTED CHLOROBIPHENYLS IN FISH AND MARINE MAMMALS

被引：36
作者：
DEBOER, J
STRONCK, CJN
VANDERVALK, F
WESTER, PG
DAUDT, MJM
机构：
[1] Netherlands Institute for Fisheries Research, 1970 AB IJmuiden
来源：
CHEMOSPHERE | 1992年 / 25卷 / 7-10期
关键词：
D O I：
10.1016/0045-6535(92)90142-E
中图分类号：
X [环境科学、安全科学];
学科分类号：
08 ; 0830 ;
摘要：
A method has been developed for the analysis of non-ortho substituted chlorobiphenyls (CBs) in fish. The method consists of a saponification, clean-up over alumina and silica and HPLC fractionation over porous graphitic carbon. GC/NCI-MS is used for the final determination. Concentration of non-ortho CBs have been measured in Aroclor 1254, several fish samples and dolphin blubber.
引用
收藏
页码：1277 / 1283
页数：7
相关论文
共 18 条
[1]   ANALYSIS OF POLYCHLORINATED-BIPHENYLS (PCB) BY GLASS-CAPILLARY GAS-CHROMATOGRAPHY - COMPOSITION OF TECHNICAL AROCLOR-PCB AND CLOPHEN-PCB MIXTURES [J].
BALLSCHMITER, K ;
ZELL, M .
FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 1980, 302 (01) :20-31
[2]   FRACTIONATION OF POLYCHLORINATED-BIPHENYLS, POLYCHLORINATED DIBENZO-PARA-DIOXINS, AND POLYCHLORINATED DIBENZOFURANS ON POROUS GRAPHITIC CARBON [J].
CREASER, CS ;
ALHADDAD, A .
ANALYTICAL CHEMISTRY, 1989, 61 (11) :1300-1302
[3]  
DEBOER J, 1989, HRC-J HIGH RES CHROM, V12, P755
[4]   TRENDS IN CHLOROBIPHENYL CONTENTS IN LIVERS OF ATLANTIC COD (GADUS-MORHUA) FROM THE NORTH-SEA, 1979-1987 [J].
DEBOER, J .
CHEMOSPHERE, 1988, 17 (09) :1811-1819
[5]  
DEBOER J, 1991, 13TH P INT S CAP CHR, P225
[6]   ISOLATION OF MONO-ORTHO AND NON-ORTHO POLYCHLORINATED-BIPHENYLS FROM BIOLOGICAL SAMPLES BY ELECTRON-DONOR ACCEPTOR HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY USING A 2-(1-PYRENYL)ETHYLDIMETHYLSILYLATED SILICA COLUMN [J].
HAGLUND, P ;
ASPLUND, L ;
JARNBERG, U ;
JANSSON, B .
CHEMOSPHERE, 1990, 20 (7-9) :887-894
[7]   DETERMINATION OF MONO-ORTHO AND NON-ORTHO COPLANAR PCBS IN FISH [J].
HONG, CS ;
BUSH, B .
CHEMOSPHERE, 1990, 21 (1-2) :173-181
[8]  
HUCKINS JN, 1980, J ASSOC OFF ANA CHEM, V63, P750
[9]   A SIMPLE METHOD FOR DETERMINING NON-ORTHO SUBSTITUTED PCBS IN KANECHLORS, AROCLORS AND ENVIRONMENTAL-SAMPLES [J].
KANNAN, N ;
TANABE, S ;
WAKIMOTO, T ;
TATSUKAWA, R .
CHEMOSPHERE, 1987, 16 (8-9) :1631-1634
[10]   TOXIC POTENTIAL OF NON-ORTHO AND MONO-ORTHO COPLANAR PCBS IN COMMERCIAL PCB PREPARATIONS - 2,3,7,8-T4 CDD TOXICITY EQUIVALENCE FACTORS APPROACH [J].
KANNAN, N ;
TANABE, S ;
TATSUKAWA, R .
BULLETIN OF ENVIRONMENTAL CONTAMINATION AND TOXICOLOGY, 1988, 41 (02) :267-276
12