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SELECTIVE HIGH-RESOLUTION PROTON NMR-SPECTRA IN SOLIDS
被引:7
|作者:
REIMER, JA
VAUGHAN, RW
机构:
[1] Division of Chemistry and Chemical Engineering, California Institute of Technology, Pasadena
关键词:
D O I:
10.1016/0009-2614(79)80481-9
中图分类号:
O64 [物理化学(理论化学)、化学物理学];
学科分类号:
070304 ;
081704 ;
摘要:
A technique is presented where double resonance pulse schemes, which remove both homonuclear and heteronuclear dipolar interactions, have been used to isolate the chemical shift spectrum of specific protons within polycrystalline solids. Proton spectra of Ca(CHO2)2 demonstrate the ability of the scheme to produce undistorted powder patterns, and the selective character of the technique is demonstrated with results from several organic solids and an absorbed system. © 1979.
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页码:163 / 165
页数:3
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