Methyl 4-(4-hydroxyphenyl)-6-methyl-2-sulfanylidene-1,2,3,4-tetrahydropyrimidine-5-carboxylate

被引:0
作者
Fathima, Nikhath [1 ]
Nagarajaiah, H. [1 ]
Begum, Noor Shahina [1 ]
机构
[1] Bangalore Univ, Dept Studies Chem, Bangalore 560001, Karnataka, India
关键词
Data-to-parameter ratio = 15.4; Mean σ(C-C) = 0.006 Å; R factor = 0.067; Single-crystal X-ray study; T = 296 K; wR factor = 0.224;
D O I
10.1107/S1600536814002888
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title molecule, C13H14N2O3S, the dihydropyrimidine ring is in a flattened sofa conformation, with the methine C atom forming the flap. The dihedral angle between the mean plane of the five essentially planar atoms of the dihydropyrimidine ring [maximum deviation = 0.056 (4) angstrom] and the benzene ring is 89.4 (2)degrees. The O atom of the carbonyl group is in a trans conformation with respect to the C=C bond of the dihydropyrimidine ring. In the crystal, N-H center dot center dot center dot O and O-H center dot center dot center dot S hydrogen bonds connect molecules, forming a two-dimensional network parallel to (001).
引用
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页码:O306 / +
页数:8
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