2-(1-Benzothiophen-2-yl)-4H-1,3,4-oxadiazin-5(6H)-one

被引:0
|
作者
Sun, Hong-Shun [1 ,2 ]
Li, Yu-Long [1 ]
Xu, Ning [1 ]
Shen, Lin-Jiang [2 ]
机构
[1] Nanjing Coll Chem Technol, Chem Engn Dept, Nanjing 210048, Jiangsu, Peoples R China
[2] Nanjing Univ Technol, Coll Sci, Nanjing 210009, Jiangsu, Peoples R China
关键词
D O I
10.1107/S1600536813033291
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title compound, C11H8N2O2S, the oxadiazinone ring is nearly planar [maximum deviation = 0.016 (4) angstrom], and is approximately coplanar with the benzothiophene ring system [dihedral angle = 3.1 (5)degrees]. In the crystal, molecules are linked by N-H center dot center dot center dot O hydrogen bonds, forming chains running along the b- axis direction.
引用
收藏
页码:O41 / +
页数:6
相关论文
共 50 条
  • [21] 2-(4H-1,2,4-Triazol-4-yl)pyrimidine
    Wang, Qian
    Wang, Sheng
    Wang, Yuan Yuan
    Wang, Ying
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2012, 68 : O53 - +
  • [22] 2-((5-(5-Methyl-2-phenyl-1H-imidazol-4-yl)-1,3,4-oxadiazol-2-yl)thio)-1-phenylethan-1-one
    Abdel-Wahab, Bakr F.
    Mabied, Ahmed F.
    Fettinger, James C.
    Hassan, Ahmed H. E.
    Farahat, Abdelbasset A.
    MOLBANK, 2023, 2023 (02)
  • [23] Synthesis of 2-[4-(2-chlorobenzyl)-3-methyl-6-oxopyridazin-1(6H)-yl]acetohydrazide
    Benchat, Nour-Eddine
    Anaflous, Abderrahmane
    Abouricha, Said
    El-Bali, Brahim
    Ramdani, Mohamed
    MOLBANK, 2007, (02)
  • [24] (5S,6R)-3,4,5,6-tetrahydro-5-methyl-6-phenyl-4-propyl-2H-1,3,4-oxadiazin-2-one
    Szczepura, LF
    Hitchcock, SR
    Nora, GP
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2004, 60 : O1467 - O1469
  • [25] Reactions of 2-(5-methyl-2-phenyl-2H-1,2,3-diazaphosphol-4-yl)-4H-1,3,2-benzodioxaphosphinin-4-one with chloral and hexafluoroacetone
    Mironov, Vladimir F.
    Ivkova, Gulnara A.
    Abdrakhmanova, Liliya M.
    Mironova, Ekaterina V.
    Krivolapov, Dmitry B.
    Konovalova, Irina V.
    MENDELEEV COMMUNICATIONS, 2011, 21 (05) : 282 - 284
  • [26] Tautomeric and ab initio studies of 5-thioxo-3H,4H-1,3,4-thiadiazolidin-2-one
    Cho, NS
    Park, CK
    Kim, HS
    Choi, ES
    Kang, SK
    BULLETIN OF THE KOREAN CHEMICAL SOCIETY, 1998, 19 (01) : 103 - 106
  • [27] 2-(1-benzyl-5-methyl-1H-imidazol-4-yl)-1,3,4-oxadiazole
    Li, Jing
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O2976 - U2993
  • [28] 2-(1-benzyl-4-methyl-1H-imidazol-5-yl)1,3,4-oxadiazole
    Li, Jing
    Zhou, Hong-Bin
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O2977 - U3002
  • [29] Photocyclodimerization of 5-Methyl-2H-pyran-3(6H)-one
    Groesch, Ljubov
    Kopf, Juergen
    Margaretha, Paul
    HELVETICA CHIMICA ACTA, 2008, 91 (12) : 2211 - 2215
  • [30] A facile synthesis of N-arylcyanoformamidoximes, 4-aryl-3-cyano-1,2,4-oxadiazin-5(6H)-ones, 2-cyanoquinazoline-3-oxides, and 2-cyanoquinazolines via 5-arylimino-4-chloro-5H-1,2,3-dithiazoles
    Chang, YG
    Kim, K
    HETEROCYCLES, 1999, 51 (11) : 2653 - 2666