3-Acetyl-1-(2-methylphenyl) thiourea

被引：26

作者：

Shahwar, Durre ^{[1
]}

Tahir, M. Nawaz ^{[2
]}

Chohan, Muhammad Mansha ^{[1
]}

Ahmad, Naeem ^{[1
]}

Raza, M. Asam ^{[3
]}

机构：

[1] Govt Coll Univ, Dept Chem, Lahore, Pakistan

[2] Univ Sargodha, Dept Phys, Sargodha, Pakistan

[3] Univ Gujrat, Dept Chem, Gujrat, Pakistan

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷

关键词：

D O I：

10.1107/S1600536812011658

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C10H12N2OS, the toluene and the Ncarbamothioylacetamide units are oriented at dihedral angle of 78.75 (5)degrees. An intramolecular N-H center dot center dot center dot O hydrogen bond generates an S(6) ring. In the crystal, molecules are linked into [101] chains by pairs of N-H center dot center dot center dot S hydrogen bonds [which generate R-2(2) (8) loops] and pairs of O-H center dot center dot center dot O hydrogen bonds [which generate R-2(2) (4) loops]. The two motifs alternate in the chain.

引用

页码：O1160 / +

页数：7

共 8 条

[1] [Anonymous], 2005, SADABS
[2] PATTERNS IN HYDROGEN BONDING - FUNCTIONALITY AND GRAPH SET ANALYSIS IN CRYSTALS
BERNSTEIN, J
DAVIS, RE
SHIMONI, L
CHANG, NL
[J]. ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 1995, 34 (15) : 1555 - 1573
[3] Bruker, 2012, APEX2 SAINT
[4] Farrugia L.J., 1997, J APPL CRYSTALLOGR, V30, P565, DOI [DOI 10.1107/S0021889897003117, 10.1107/S0021889897003117]
[5] Farrugia L.J., 1999, J APPL CRYSTALLOGR, V32, P837, DOI [10.1107/S0021889812029111, DOI 10.1107/S0021889812029111]
[6] 3-Acetyl-1-phenylthiourea
Shahwar, Durre
Tahir, M. Nawaz
Chohan, Muhammad Mansha
Ahmad, Naeem
Samiullah
[J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2012, 68 : O508 - U1600
[7] A short history of SHELX
Sheldrick, George M.
[J]. ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 : 112 - 122
[8] Structure validation in chemical crystallography
Spek, Anthony L.
[J]. ACTA CRYSTALLOGRAPHICA SECTION D-STRUCTURAL BIOLOGY, 2009, 65 : 148 - 155

← 1 →