Determination of polycyclic aromatic hydrocarbons in processed foods

被引:5
作者
Hu, Soojung [1 ]
Jin, Sunhee [1 ]
Lee, Kwangho [1 ]
Choi, Dongmi [1 ]
机构
[1] Natl Inst Food & Drug Safety Evaluat, Food Safety Evaluat Dept, 194 Tongil Ro, Seoul 122704, South Korea
关键词
Polycyclic aromatic hydrocarbons; benzo(a) pyrene; processed food; HPLC/FLD;
D O I
10.5806/AST.2010.23.2.196
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
In this study, the following concentrations of some PAHs (Polycyclic Aromatic Hydrocarbons) were investigated; [benzo(a) anthracene, chrysene, benzo(b) fluoranthene, benzo(k) fluoranthene, benzo(a) pyrene, dibenzo(a, h) anthracene, benzo(g,h,i) perylene, indeno(1,2,3-c,d) pyrene] in processed foods (n=165) and cooked meats (n=45) and established the analytical method by characteristics of processed foods. The methodology involved extraction (alkali digestion, liquid-liquid extraction, microwave extraction), clean-up on Sep-Pak Florisil Cartridges and determination by HPLC/FLD (High Performance Liquid Chromatography/Fluorescence Detector). The recovery of overall method for 8 PAHs spiked into these products ranged from 92 to 103%. The mean level of detected foods was found to be benzo(b) fluoranthene 0.9 mu g/kg in smoked salmon, benzo(b) fluoranthene 1.0 mu g/kg, benzo(k) fluoranthene 0.3 mu g/kg, benzo(a) pyrene 0.9 mu g/kg in dried banana, benzo(b) fluoranthene 0.2 mu g/kg, benzo(k) fluoranthene 0.1 mu g/kg, benzo(a) pyrene 0.2 mu g/kg in smoked chicken, benzo(b) fluoranthene 1.3 mu g/kg, benzo(k) fluoranthene 0.3 mu g/kg, benzo(a) pyrene 0.9 mu g/kg in charcoal grilled pork, respectively.
引用
收藏
页码:196 / 204
页数:9
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