ANALYSIS OF MINOR COMPONENTS BY ULTRAHIGH RESOLUTION NMR .2. DETECTION OF 0.01-PERCENT DIACETONE ALCOHOL IN PURE ACETONE AND DIRECT MEASUREMENT OF THE RATE OF THE ALDOL CONDENSATION OF ACETONE

被引：18

作者：

MAPLE, SR ^{[1
]}

ALLERHAND, A ^{[1
]}

机构：

[1] INDIANA UNIV, DEPT CHEM, BLOOMINGTON, IN 47405 USA

来源：

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY | 1987年 / 109卷 / 22期

关键词：

D O I：

10.1021/ja00256a008

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

引用

页码：6609 / 6614

页数：6

共 41 条

[1] Decomposition of diacetone alcohol by weaker bases [J].

Akerlof, G .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1928, 50 :733-744

[2] Decomposition of diacetone alcohol in alkali hydroxide solutions [J].

Akerlof, G .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1927, 49 :2955-2981

[3] Decomposition of diacetone alcohol in alkali hydroxide-alkali salt solutions [J].

Akerlof, G .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1926, 48 :3046-3063

[4] ULTRA-HIGH-RESOLUTION NMR .5. 0.003 HZ INSTRUMENTAL BROADENING AND IMPROVED LINESHAPE IN A 10 MM C-13 PROBE [J].

ALLERHAND, A ;

BRADLEY, CH .

JOURNAL OF MAGNETIC RESONANCE, 1986, 67 (01) :173-176

[5] ULTRA-HIGH-RESOLUTION NMR .3. PERFORMANCE OF WALTZ-16 PROTON DECOUPLING [J].

ALLERHAND, A ;

ADDLEMAN, RE ;

OSMAN, D ;

DOHRENWEND, M .

JOURNAL OF MAGNETIC RESONANCE, 1985, 65 (02) :361-363

[6] ULTRAHIGH RESOLUTION NMR .1. GENERAL-CONSIDERATIONS AND PRELIMINARY-RESULTS FOR C-13 NMR [J].

ALLERHAND, A ;

ADDLEMAN, RE ;

OSMAN, D .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1985, 107 (20) :5809-5810

[7] NATURAL ABUNDANCE CARBON-13 PARTIALLY RELAXED FOURIER TRANSFORM NUCLEAR MAGNETIC RESONANCE SPECTRA OF COMPLEX MOLECULES [J].

ALLERHAND, A ;

DODDRELL, D ;

KOMOROSKI, R .

JOURNAL OF CHEMICAL PHYSICS, 1971, 55 (01) :189-+

[8] ULTRAHIGH RESOLUTION NMR .2. MEASUREMENTS OF SECONDARY ISOTOPE EFFECTS ON CHEMICAL-SHIFTS, LONG-RANGE CARBON-CARBON SCALAR COUPLING-CONSTANTS, AND C-13 SPIN-SPIN RELAXATION-TIMES DIRECTLY FROM LINE WIDTHS [J].

ALLERHAND, A ;

DOHRENWEND, M .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1985, 107 (23) :6684-6688

[9] TRITIUM ISOTOPE EFFECTS ON C-13 NMR CHEMICAL-SHIFTS [J].

ARROWSMITH, CH ;

BALTZER, L ;

KRESGE, AJ ;

POWELL, MF ;

TANG, YS .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1986, 108 (06) :1356-1357

[10] MINIMIZATION OF NUCLEAR MAGNETIC-RESONANCE SPINNING SIDEBANDS BY SPINNING RATE MODULATION [J].

BAMMEL, B ;

EVILIA, RF .

ANALYTICAL CHEMISTRY, 1980, 52 (12) :1999-2000

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