METHOD FOR THE DETERMINATION OF CHLORDECONE (KEPONE) IN HUMAN-SERUM AND BLOOD

被引：3
|
作者：
CAPLAN, YH [1 ]
THOMPSON, BC [1 ]
HEBB, JH [1 ]
机构：
[1] UNIV MARYLAND,DEPT PATHOL,DIV FORENS PATHOL,BALTIMORE,MD 21201
来源：
JOURNAL OF ANALYTICAL TOXICOLOGY | 1979年 / 3卷 / 05期
关键词：
D O I：
10.1093/jat/3.5.202
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
A simple method for the determination of chlordecone in serum and blood employing selective separation and extraction using benzene is presented. The extracted pesticide is analyzed quantitatively by gas chromatography using an electron capture detector and a 10% DC-200 on 100/120 mesh Gas-Chrom Q column. The method is sensitive to a concentration of 10 μg/llter In a l-mL sample and Is highly reproducible showing a within-run coefficient of variation (CV) of 4.1% and an out-of-run CV of 6.9%. © 1979 Oxford University Press.
引用
收藏
页码：202 / 205
页数：4
相关论文
共 50 条
  • [21] UTILIZATION OF ABELL METHOD FOR THE DETERMINATION OF CHOLESTEROL AND ITS OXIDES IN HUMAN-SERUM
    POLYCHRONOPOULOS, E
    DELICONSTANTINOS, G
    TRICHOPOULOU, A
    CELLULAR AND MOLECULAR BIOLOGY, 1988, 34 (04) : 383 - 386
  • [22] IMPROVED METHOD FOR THE DETERMINATION OF SULFATE IN HUMAN-SERUM USING ION CHROMATOGRAPHY
    REITER, C
    MULLER, S
    MULLER, T
    JOURNAL OF CHROMATOGRAPHY-BIOMEDICAL APPLICATIONS, 1987, 413 : 251 - 256
  • [23] A SELECTIVE AND SENSITIVE METHOD FOR THE DETERMINATION OF PROPAFENON AND METABOLITES IN HUMAN-SERUM BY HPLC
    BEUMAN, G
    BOESTEN, M
    VANDERHEIJDEN, J
    PHARMACEUTISCH WEEKBLAD-SCIENTIFIC EDITION, 1986, 8 (06) : 319 - 319
  • [24] THIN-LAYER CHROMATOGRAPHIC METHOD FOR DETERMINATION OF DIGITOXIN IN HUMAN-SERUM
    FABER, DB
    DEKOK, A
    JOURNAL OF CHROMATOGRAPHY, 1977, 143 (01): : 95 - 103
  • [25] GAS-CHROMATOGRAPHIC METHOD FOR DETERMINATION OF AMITRIPTYLINE AND NORTRIPTYLINE IN HUMAN-SERUM
    JORGENSEN, A
    ACTA PHARMACOLOGICA ET TOXICOLOGICA, 1974, 35 : 34 - 34
  • [26] GAS-CHROMATOGRAPHIC METHOD FOR DETERMINATION OF AMITRIPTYLINE AND NORTRIPTYLINE IN HUMAN-SERUM
    JORGENSEN, A
    ACTA PHARMACOLOGICA ET TOXICOLOGICA, 1975, 36 (01): : 79 - 90
  • [27] METHOD FOR DETERMINATION OF CHLORPROMAZINE IN HUMAN BLOOD SERUM
    CHRISTOPH, GW
    DAVIS, JM
    SCHMIDT, DE
    JANOWSKY, DS
    CLINICA CHIMICA ACTA, 1972, 38 (02) : 265 - +
  • [28] DETERMINATION OF CIRCULATING ELASTIN PEPTIDES IN HUMAN-SERUM
    BAYDANOFF, SI
    NICOLOFF, GA
    DOKLADI NA BOLGARSKATA AKADEMIYA NA NAUKITE, 1986, 39 (06): : 85 - 87
  • [29] DETERMINATION OF QUINIDINE IN HUMAN-SERUM IN PRESENCE OF DIURETICS
    OSINGA, A
    DEWOLFF, FA
    CLINICA CHIMICA ACTA, 1976, 73 (03) : 505 - 512
  • [30] DETERMINATION OF SOME HYDROXYCHOLESTEROLS IN HUMAN-SERUM SAMPLES
    KOOPMAN, BJ
    VANDERMOLEN, JC
    WOLTHERS, BG
    VANDERPAS, JB
    JOURNAL OF CHROMATOGRAPHY-BIOMEDICAL APPLICATIONS, 1987, 416 (01): : 1 - 13
12345