METHOD FOR THE DETERMINATION OF CHLORDECONE (KEPONE) IN HUMAN-SERUM AND BLOOD

被引：3
|
作者：
CAPLAN, YH [1 ]
THOMPSON, BC [1 ]
HEBB, JH [1 ]
机构：
[1] UNIV MARYLAND,DEPT PATHOL,DIV FORENS PATHOL,BALTIMORE,MD 21201
来源：
JOURNAL OF ANALYTICAL TOXICOLOGY | 1979年 / 3卷 / 05期
关键词：
D O I：
10.1093/jat/3.5.202
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
A simple method for the determination of chlordecone in serum and blood employing selective separation and extraction using benzene is presented. The extracted pesticide is analyzed quantitatively by gas chromatography using an electron capture detector and a 10% DC-200 on 100/120 mesh Gas-Chrom Q column. The method is sensitive to a concentration of 10 μg/llter In a l-mL sample and Is highly reproducible showing a within-run coefficient of variation (CV) of 4.1% and an out-of-run CV of 6.9%. © 1979 Oxford University Press.
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页码：202 / 205
页数：4
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