COHERENCE SELECTION BY GRADIENTS WITHOUT SIGNAL ATTENUATION - APPLICATION TO THE 3-DIMENSIONAL HNCO EXPERIMENT

被引：245

作者：

SCHLEUCHER, J ^{[1
]}

SATTLER, M ^{[1
]}

GRIESINGER, C ^{[1
]}

机构：

[1] UNIV FRANKFURT,INST ORGAN CHEM,MARIE CURIE STR 11,D-60439 FRANKFURT,GERMANY

来源：

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH | 1993年 / 32卷 / 10期

关键词：

D O I：

10.1002/anie.199314891

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Maximum sensitivity and excellent suppression of the water signal is achieved in 3D triple‐resonance NMR experiments by the application of a heteronuclear gradient echo in phase‐modulating pulse sequences. This principle is demonstrated for an HNCO experiment applied to a complex of a uniformly 13C/15Nlabeled protein (calmodulin) and a peptide (C2OW). Copyright © 1993 by VCH Verlagsgesellschaft mbH, Germany

引用

页码：1489 / 1491

页数：3

共 28 条

[1] PULSED FIELD GRADIENTS IN NMR - AN ALTERNATIVE TO PHASE CYCLING
BARKER, P
FREEMAN, R
[J]. JOURNAL OF MAGNETIC RESONANCE, 1985, 64 (02) : 334 - 338
[2] SEPARATION OF THE DIFFERENT ORDERS OF NMR MULTIPLE-QUANTUM TRANSITIONS BY THE USE OF PULSED FIELD GRADIENTS
BAX, A
DEJONG, PG
MEHLKOPF, AF
SMIDT, J
[J]. CHEMICAL PHYSICS LETTERS, 1980, 69 (03) : 567 - 570
[3] SELECTION OF COHERENCE-TRANSFER PATHWAYS IN NMR PULSE EXPERIMENTS
BODENHAUSEN, G
KOGLER, H
ERNST, RR
[J]. JOURNAL OF MAGNETIC RESONANCE, 1984, 58 (03) : 370 - 388
[4] THE GENERATION OF PHASE-SENSITIVE 2D N-15-H-1 SPECTRA USING GRADIENT PULSES FOR COHERENCE-TRANSFER-PATHWAY SELECTION
BOYD, J
SOFFE, N
JOHN, B
PLANT, D
HURD, R
[J]. JOURNAL OF MAGNETIC RESONANCE, 1992, 98 (03): : 660 - 664
[5] SENSITIVITY IMPROVEMENT IN PROTON-DETECTED 2-DIMENSIONAL HETERONUCLEAR RELAY SPECTROSCOPY
CAVANAGH, J
PALMER, AG
WRIGHT, PE
RANCE, M
[J]. JOURNAL OF MAGNETIC RESONANCE, 1991, 91 (02) : 429 - 436
[6] RAPID ACQUISITION OF 3-DIMENSIONAL TRIPLE-RESONANCE EXPERIMENTS USING PULSED FIELD GRADIENT TECHNIQUES
DAVIS, AL
BOELENS, R
KAPTEIN, R
[J]. JOURNAL OF BIOMOLECULAR NMR, 1992, 2 (04) : 395 - 400
[7] ABSORPTION-MODE 2-DIMENSIONAL NMR-SPECTRA RECORDED USING PULSED FIELD GRADIENTS
DAVIS, AL
LAUE, ED
KEELER, J
MOSKAU, D
LOHMAN, J
[J]. JOURNAL OF MAGNETIC RESONANCE, 1991, 94 (03): : 637 - 644
[8] GAUSSIAN PULSE CASCADES - NEW ANALYTICAL FUNCTIONS FOR RECTANGULAR SELECTIVE INVERSION AND IN-PHASE EXCITATION IN NMR
EMSLEY, L
BODENHAUSEN, G
[J]. CHEMICAL PHYSICS LETTERS, 1990, 165 (06) : 469 - 476
[9] IMPROVED 3D TRIPLE-RESONANCE NMR TECHNIQUES APPLIED TO A 31-KDA PROTEIN
GRZESIEK, S
BAX, A
[J]. JOURNAL OF MAGNETIC RESONANCE, 1992, 96 (02): : 432 - 440
[10] GRADIENT-ENHANCED PROTON-DETECTED HETERONUCLEAR MULTIPLE-QUANTUM COHERENCE SPECTROSCOPY
HURD, RE
JOHN, BK
[J]. JOURNAL OF MAGNETIC RESONANCE, 1991, 91 (03): : 648 - 653

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