STRUCTURE OF DIETHYL 5,11,17,23-TETRA-TERT-BUTYL-26,28-BIS(2-METHOXYETHOXY)-CALIX[4]ARENE-25,27-BIS(OXYACETATE)

被引：6
|
作者：
GUELZIM, A [1 ]
KHRIFI, S [1 ]
BAERT, F [1 ]
ASFARI, Z [1 ]
VICENS, J [1 ]
机构：
[1] ECOLE EUROPEENNE HAUTES ETUDES IND CHIM STRASBOURG,CHIM ANALYT & MINERALE LAB,CNRS,URA 405,F-67008 STRASBOURG,FRANCE
来源：
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 1993年 / 49卷
关键词：
D O I：
10.1107/S010827019300349X
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
We present here the synthesis and X-ray crystal structure of a new 2 + 2' modified p-tert-butylcalix[4]arene, diethyl {5,11,17,23-tetra-tert-butyl-26,28-bis-(2-methoxyethoxy)pentacyclo[19.3.1. 1(3,7). 1(9,13).1(15,19)]-octacosa-1(25),3,5,7(28),9,11,13(27),15,17,19(26),-21,23-dodecaene-25,27-diyldioxy}diacetate, bearing glycol methyl ether and ethyl ester functional groups. H-1 NMR spectra of this compound indicated that it has a cone conformation; this is confirmed by the crystallographic study.
引用
收藏
页码：2121 / 2124
页数：4
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