DESIGN AND APPLICATION OF A REFLUX MODIFICATION FOR THE SYNTHESIS OF ORGANOMETALLIC COMPOUNDS USING MICROWAVE DIELECTRIC LOSS HEATING EFFECTS

被引：60

作者：

BAGHURST, DR ^{[1
]}

MINGOS, DMP ^{[1
]}

机构：

[1] UNIV OXFORD,INORGAN CHEM LAB,OXFORD OX1 3QR,ENGLAND

来源：

JOURNAL OF ORGANOMETALLIC CHEMISTRY | 1990年 / 384卷 / 03期

关键词：

D O I：

10.1016/0022-328X(90)87135-Z

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

A commercially available microwave oven has been modified so that syntheses involving the refluxing of organic solvents can be safely and conveniently undertaken. The applications of this technique for accelerating the rates of reactions leading to the synthesis of some commonly used organometallic and coordination compounds are described. © 1990.

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页码：C57 / C60

页数：4

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