Crystal structure of 1-(4-formylbenzylidene)-4-methylthiosemicarbazone

被引：0
|
作者：
Pino-Cuevas, Arantxa [1 ]
Carballo, Rosa [1 ]
Vazquez-Lopez, Ezequiel M. [1 ]
机构：
[1] Univ Vigo, Fac Quim Edificio Ciencias Expt, Dept Quim Inorgan, E-36310 Vigo, Spain
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2014年 / 70卷
关键词：
crystal structure; thiosemicarbazone; thiourea; hydrogen bonding;
D O I：
10.1107/S1600536814016407
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The structure of the title compound, C10H11N3OS, comprises an approximately planar molecule, with the r.m.s. deviation for the 15 non-H atoms being 0.089 angstrom. The conformation about the imine bond is E and an intramolecular N-H...N hydrogen bond is evident. Molecules are linked into a supramolecular chain along the b axis by N-H...S hydrogen bonds.
引用
收藏
页码：O926 / +
页数：6
相关论文
共 50 条
  • [1] Crystal structure of 1-(4-formylbenzylidene)thiosemicarbazone
    Carballo, Rosa
    Pino-Cuevas, Arantxa
    Vazquez-Lopez, Ezequiel M.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : O970 - +
  • [2] Crystal structure of 3-methylpyridine-2-carbaldehyde 4-methylthiosemicarbazone monohydrate
    Mokhtaruddin, Nur Shuhada Mohd
    Ravoof, Thahira Begum S. A.
    Tahir, Mohamed Ibrahim Mohamed
    Tiekink, Edward R. T.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : O253 - U366
  • [3] Crystal structure of 4-hydroxy-3-methoxybenzaldehyde 4-methylthiosemicarbazone methanol monosolvate
    de Oliveira, Adriano Bof
    Beck, Johannes
    Landvogt, Christian
    Santos Feitosa, Barbara Regina
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : O313 - U421
  • [4] Crystal structure and photoisomerism of 1-phenyl-3-methyl-4-(4-fluorobenzal)-5-pyrazolone 4-methylthiosemicarbazone in the solid state
    Zhong, Yuting
    Liu, Lang
    Liu, Guangfei
    Wu, Dongling
    Guo, Jixi
    Jia, Dianzeng
    JOURNAL OF MOLECULAR STRUCTURE, 2008, 889 (1-3) : 259 - 264
  • [5] 2,4-Dichlorobenzaldehyde 4-methylthiosemicarbazone
    Li, Rongchun
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O20 - U1482
  • [6] Synthesis and Crystal Structure of 4-Formaldehyde Benzaldehyde Methylthiosemicarbazone
    Su, Wei
    Qian, Quanquan
    He, Chunling
    Liu, Lifeng
    Zhou, Quan
    Li, Peiyuan
    ASIAN JOURNAL OF CHEMISTRY, 2013, 25 (14) : 8211 - 8212
  • [7] SYNTHESIS AND CRYSTAL STRUCTURE OF 1-(4-FLUOROPHENYL)- AND 1-(4-DIMETHYLAMINO)PHENYLGERMATRANES
    Lukevics, E.
    Ignatovich, L.
    Shul'ga, T.
    Belyakov, S.
    CHEMISTRY OF HETEROCYCLIC COMPOUNDS, 2008, 44 (05) : 615 - 620
  • [8] Synthesis and crystal structure of 1-(4-fluorophenyl)-and 1-(4-dimethylamino)phenylgermatranes
    E. Lukevics
    L. Ignatovich
    T. Shul’ga
    S. Belyakov
    Chemistry of Heterocyclic Compounds, 2008, 44 : 615 - 620
  • [9] Crystal structure of 1-(4-methylphenyl)-3-(propan-2-ylideneamino)thiourea
    Jotani, Mukesh M.
    Yeo, Chien Ing
    Tiekink, Edward R. T.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : 1236 - +
  • [10] Crystal structure of 1-[(4-methylbenzene)sulfonyl]pyrrolidine
    Stenfors, Brock A.
    Staples, Richard J.
    Biros, Shannon M.
    Ngassa, Felix N.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2020, 76 : 452 - +
12345