Tris(ethylenediamine-kappa N-2,N ')nickel(II) bis(dimethyl phosphate)

被引:2
作者
Rafizadeh, Masoud [1 ]
Moshtaghin, Hamid Reza Saadati [1 ]
Amani, Vahid [1 ]
机构
[1] Islamic Azad Univ, Dept Chem, Share Ray Branch, Tehran, Iran
来源
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷
关键词
data-to-parameter ratio = 18.3; mean σ(C-C) = 0.003 Å; R factor = 0.034; single-crystal X-ray study; T = 120 K; wR factor = 0.085;
D O I
10.1107/S1600536812029984
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title compound, [Ni(C2H8N2)(3)][O2P(OCH3)(2)](2), the Ni-II atom is six-coordinated in a distorted octahedral geometry by six N atoms from three ethylenediamine ligands. The P atoms of the anions adopt a distorted tetrahedral geometry. In the crystal, intermolecular N-H center dot center dot center dot O and C-H center dot center dot center dot O hydrogen bonds link the cations and anions into a three-dimensional network.
引用
收藏
页码:M1032 / U295
页数:9
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