USE OF RADIO-GAS CHROMATOGRAPHY AND TRITIUM LABEL TO OPTIMIZE DERIVATIZATION PROCEDURES

被引:2
作者
BABA, S
AKIRA, K
SEYAMA, Y
机构
[1] Tokyo College of Pharmacy, Hachioji, Tokyo, 192-03
来源
JOURNAL OF CHROMATOGRAPHY-BIOMEDICAL APPLICATIONS | 1990年 / 530卷 / 01期
关键词
D O I
10.1016/S0378-4347(00)82296-3
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A sensitive determination of gas chromatographic peak yields by a new radio-gas chromatograph equipped with a synchronized accumulating radioisotope detector is described. Peak yields could be easily determined by the radio-gas chromatograph using [3H]hexadecane or [3H]androstenedione as a standard substance. The usefulness of the determination of peak yields was demonstrated by optimizing the derivatization conditions of 6-keto-prostaglandin F1. © 1990.
引用
收藏
页码:1 / 9
页数:9
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