4-[5-(4-Chlorophenyl)-3-methyl-1H-pyrazol-1-yl]benzenesulfonamide

被引：0
|
作者：
Farrukh, Muhammad A. [1 ]
Mohamed, Shaaban K. [2 ,3 ]
Ahmed, Maqsood [1 ]
Marzouk, Adel A. [4 ]
El-Moghazy, Samir M. [5 ]
机构：
[1] Govt Coll Univ, Dept Chem, Lahore 54000, Pakistan
[2] Manchester Metropolitan Univ, Chem & Environm Div, Manchester M1 5GD, Lancs, England
[3] Menia Univ, Fac Sci, Chem Dept, El Minia, Egypt
[4] Al Azhar Univ, Fac Sci, Pharmaceut Chem Dept, Cairo, Egypt
[5] Cairo Univ, Fac Pharm, Pharmaceut Chem Dept, Cairo, Egypt
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2013年 / 69卷
关键词：
data-to-parameter ratio = 16.0; mean σ(C-C) = 0.004 Å; R factor = 0.041; single-crystal X-ray study; T = 296 K; wR factor = 0.115;
D O I：
10.1107/S1600536813002134
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, C16H14ClN3O2S, the dihedral angle between the benzene and pyrazole rings is 52.75 (2)degrees, while that between the pyrazole and 4-chlorophenyl rings is 54.0 (3)degrees. The terminal sulfonamide group adopts an approximately tetrahedral geometry about the S atom with a C - S - N angle of 108.33 (10)degrees. In the crystal, pairs of N-H center dot center dot center dot N hydrogen bonds lead to the formation of inversion dimers. These dimers are linked via a second pair of N-H center dot center dot center dot N hydrogen bonds and C-H center dot center dot center dot O interactions, forming a two-dimensional network lying parallel to the bc plane. The two-dimensional networks are linked via C-H center dot center dot center dot Cl interactions, forming a three-dimensional structure.
引用
收藏
页码：O295 / +
页数：11
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