Synthesis and Characterization of L-alanine based Poly(ester-amide)s

被引：0

作者：

Marwa, Abbes ^{[1
]}

Slim, Salhi ^{[1
]}

Christelle, Delaite ^{[2
]}

Souhir, Abid ^{[1
]}

Rachid, El-Gharbi ^{[1
]}

机构：

[1] Univ Sfax, Fac Sci, Lab Chim Appl HCGP, Sfax 3000, Tunisia

[2] Univ Haute Alsace, Lab Photochim & Ingn Macromol, Mulhouse, France

来源：

JOURNAL OF NEW TECHNOLOGY AND MATERIALS | 2016年 / 6卷 / 01期

关键词：

Adipic acid; L-alanine; melt polycondensation; microstructure; NMR; Poly(ester-amide);

D O I：

暂无

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Novel biomaterials L-alanine based poly(ester-amide)s (PEAs) differing in the amide/ester ratio have been directly synthesized by direct melt copolycondensation of Adipic acid, L-alanine and various aliphatic and heterocyclic diols. PEAs were systematically characterized with intrinsic viscosity, FTIR, H-1-NMR, C-13-NMR, DSC and SEC measurements. The resulting copolymers are amorphous and present increasing glass transition temperatures at increasing L-Alanine contents. L-Alanine-PEAs proved to be materials having high molecular weights that could reach 41800 g/mol.

引用

页码：49 / 59

页数：11

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