Crystal structure and Hirshfeld surface analysis of (E)-N-[(2-ethoxynaphthalen-1-yl)methylidene]-5,6,7,8-tetrahydronapntnalen-1-amine

被引:8
作者
Kansiz, Sevgi [1 ]
Macit, Mustafa [2 ]
Dege, Necmi [1 ]
Tsapyuk, Galyna G. [3 ]
机构
[1] Ondokuz Mayis Univ, Fac Arts & Sci, Dept Phys, TR-55139 Samsun, Turkey
[2] Ondokuz Mayis Univ, Fac Arts & Sci, Dept Chem, TR-55139 Samsun, Turkey
[3] OO Bohomolets Natl Med Univ, Dept Gen Chem, Shevchenko Blvd 13, UA-01601 Kiev, Ukraine
关键词
crystal structure; Schiff base; Hirshfeld surface;
D O I
10.1107/S2056989018013117
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title Schiff base compound, C23H23NO, the two ring systems are twisted by 51.40 (11)degrees relative to each other. In the crystal, the molecules are connected by weak C-H center dot center dot center dot pi interactions, generating a three-dimensional supramolecular structure. Hirshfeld surface analysis and two-dimensional fingerprint plots indicate that the most important contributions to the crystal packing are from H center dot center dot center dot H (67.2%), C center dot center dot center dot H/H center dot center dot center dot C (26.7%) and C center dot center dot center dot C (2.5%) interactions.
引用
收藏
页码:1513 / +
页数:10
相关论文
共 17 条
[11]   Regular High-Nuclearity Species from Square Building Blocks: A Triangular 3 x [2 x 2] Ni12 Complex Generated by the Self-assembly of Three [2 x 2] Ni4 Molecular Grids [J].
Moroz, Yurii S. ;
Demeshko, Serhiy ;
Haukka, Matti ;
Mokhir, Andriy ;
Mitra, Utpal ;
Stocker, Michael ;
Mueller, Paul ;
Meyer, Franc ;
Fritsky, Igor O. .
INORGANIC CHEMISTRY, 2012, 51 (14) :7445-7447
[12]   Crystal structure and Hirshfeld surface analysis of 4-[4-(1H-benzo[d] imidazol-2-yl)phenoxy]phthalo-nitrile monohydrate [J].
Sen, Pinar ;
Kansiz, Sevgi ;
Dege, Necmi ;
Iskenderov, Turganbay S. ;
Yildiz, S. Zeki .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2018, 74 :994-+
[13]  
Sheldrick GM, 2015, ACTA CRYSTALLOGR C, V71, P3, DOI [10.1107/S2053229614024218, 10.1107/S0108767307043930]
[14]   Structure validation in chemical crystallography [J].
Spek, Anthony L. .
ACTA CRYSTALLOGRAPHICA SECTION D-STRUCTURAL BIOLOGY, 2009, 65 :148-155
[15]  
Stoe & Cie, 2002, X AREA XRED32
[16]  
Turner M. J., 2017, CRYSTAL EXPLORER17 5
[17]   Direct Access to Enantioenriched Spiroacetals through Asymmetric Relay Catalytic Three-Component Reaction [J].
Wu, Hua ;
He, Yu-Ping ;
Gong, Liu-Zhu .
ORGANIC LETTERS, 2013, 15 (03) :460-463