X-RAY STRUCTURAL STUDY OF (ETA-5-C5H5)2W2OS(CO)7[MU-3-MEC6H4C=CC6H4ME] - AN UNUSUAL EXAMPLE OF 2 ISOMERS OF A COMPLEX IN AN ORDERED SINGLE-CRYSTAL

被引：32
作者：
CHURCHILL, MR
BUENO, C
WASSERMAN, HJ
机构：
来源：
INORGANIC CHEMISTRY | 1982年 / 21卷 / 02期
关键词：
D O I：
10.1021/ic00132a035
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
引用
收藏
页码：640 / 644
页数：5
相关论文
共 15 条
[1]   MOLECULAR-STRUCTURES AND BARRIERS TO INTERNAL-ROTATION IN BIS(-ETA5-CYCLOPENTADIENYL)HEXACARBONYLDITUNGSTEN AND ITS MOLYBDENUM ANALOG [J].
ADAMS, RD ;
COLLINS, DM ;
COTTON, FA .
INORGANIC CHEMISTRY, 1974, 13 (05) :1086-1090
[2]  
[Anonymous], 1974, INT TABLES XRAY CRYS, VIV, p[99, 149]
[3]   CHEMISTRY OF DI-METAL AND TRI-METAL COMPLEXES WITH BRIDGING CARBENE OR CARBYNE LIGANDS .8. SYNTHESIS OF THE TRIMETAL COMPOUNDS [NI(W(MU-CC6H4ME-4)(CO)2(ETA-C5H5)]2], [PD(W(MU-CC6H4ME-4)(CO)2(ETA-C5H5)]2], [PT(W(MU-CC6H4ME-4)(CO)2(ETA-C5H5)]2] AND CRYSTAL-STRUCTURES OF THE PLATINUM AND NICKEL-COMPLEXE(W [J].
ASHWORTH, TV ;
CHETCUTI, MJ ;
HOWARD, JAK ;
STONE, FGA ;
WISBEY, SJ ;
WOODWARD, P .
JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1981, (03) :763-770
[4]   ADDITION OF NUCLEOPHILIC METAL-COMPLEXES TO MONONUCLEAR TRANSITION-METAL CARBYNE COMPOUNDS - X-RAY CRYSTAL-STRUCTURE OF [PTW(MU-CC6H4-PARA-ME)(CO)2(PME2PH)2(ETA-C5H5)] [J].
ASHWORTH, TV ;
HOWARD, JAK ;
STONE, FGA .
JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1979, (01) :42-43
[5]   STRUCTURAL STUDIES ON SOME (ETA-5-C5H5)M(CO)3XMOLECULES - (ETA-5-C5H5)W(CO)3CL,(ETA-5-C5H5)MO(CO)3CL, AND (ETA-5-C5H5)MO(CO)3HGCL [J].
BUENO, C ;
CHURCHILL, MR .
INORGANIC CHEMISTRY, 1981, 20 (07) :2197-2202
[6]   POLYNUCLEAR TUNGSTEN-IRON, TUNGSTEN-RUTHENIUM AND TUNGSTEN-OSMIUM CARBONYL-COMPLEXES - CRYSTAL-STRUCTURES OF [FEW2(MU-3-C2R2)(CO)6(ETA-C5H5)2], [OSW2(MU-3-C2R2)(CO)7-(ETA-C5H5)2] (2 ISOMERS), AND [OS3W(MU-3-CR)(CO)11(ETA-C5H5)] (R = C6H4ME-4) [J].
BUSETTO, L ;
GREEN, M ;
HOWARD, JAK ;
HESSNER, B ;
JEFFERY, JC ;
MILLS, RM ;
STONE, FGA ;
WOODWARD, P .
JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1981, (21) :1101-1103
[7]   STRUCTURAL STUDIES ON POLYNUCLEAR OSMIUM CARBONYL HYDRIDES .9. MOLECULAR-GEOMETRY OF (MU-H)3OS3W(CO)11(ETA5-C5H5) INCLUDING SOME COMMENTS ON THE POSITIONS OF MU-HYDRIDE LIGANDS IN TETRANUCLEAR METAL CLUSTERS [J].
CHURCHILL, MR ;
HOLLANDER, FJ .
INORGANIC CHEMISTRY, 1979, 18 (01) :161-166
[8]   STRUCTURAL STUDIES ON POLYNUCLEAR OSMIUM CARBONYL HYDRIDES .10. MOLECULAR-GEOMETRY AND COMMENTS ON THE LOCATION OF THE MU-2-HYDRIDE LIGAND IN (MU-H)OS3W(CO)12(ETA-5-C5H5) [J].
CHURCHILL, MR ;
HOLLANDER, FJ .
INORGANIC CHEMISTRY, 1979, 18 (03) :843-848
[9]   STRUCTURAL STUDIES ON POLYNUCLEAR OSMIUM CARBONYL HYDRIDES .1. CRYSTAL-STRUCTURES OF ISOMORPHOUS SPECIES H2OS3(CO)11 AND OS3(CO)12 - DIRECT INFORMATION ON ROLE OF AN EQUATORIAL MU-2-BRIDGING HYDRIDE LIGAND IN PERTURBING ARRANGEMENT OF CARBONYL LIGANDS IN A TRIANGULAR CLUSTER [J].
CHURCHILL, MR ;
DEBOER, BG .
INORGANIC CHEMISTRY, 1977, 16 (04) :878-884
[10]   CRYSTAL-STRUCTURE AND MOLECULAR-GEOMETRY OF DIMERIC AZULENEMANGANESE TRICARBONYL,[(C10H8)MN(CO)3]2 [J].
CHURCHILL, MR ;
LASHEWYCZ, RA ;
ROTELLA, FJ .
INORGANIC CHEMISTRY, 1977, 16 (02) :265-271
12