Ethyl 2-(5-methoxy-2-methyl-1H-indol-3yl)acetate

被引:3
作者
Mohamed, Shaaban K. [1 ,2 ]
Mague, Joel T. [3 ]
Akkurt, Mehmet [4 ]
Hassan, Alaa A. [2 ]
Albayati, Mustafa R. [5 ]
机构
[1] Manchester Metropolitan Univ, Chem & Environm Div, Manchester M1 5GD, Lancs, England
[2] Mini Univ, Fac Sci, Chem Dept, El Menia 61519, Egypt
[3] Tulane Univ, Dept Chem, New Orleans, LA 70118 USA
[4] Erciyes Univ, Fac Sci, Dept Phys, TR-38039 Kayseri, Turkey
[5] Kirkuk Univ, Coll Sci, Dept Chem, Kirkuk, Iraq
关键词
data-to-parameter ratio = 19.8; meanω(C - C) = 0.002 A °; Rfactor = 0.044; single-crystal X-ray study; T = 150 K; wRfactor = 0.117;
D O I
10.1107/S1600536813018618
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title compound, C14H17NO3, the nine-membered 1Hindole ring system is essentially planar [maximum deviation = 0.019 (1) angstrom]. In the crystal, molecules are linked via NH center dot center dot center dot O hydrogen bonds, forming chains along [001]. These chains are linked via C-H center dot center dot center dot O hydrogen bonds and CH center dot center dot center dot pi interactions, forming a two- dimensional network lying parallel to the ac plane.
引用
收藏
页码:O1242 / +
页数:7
相关论文
共 9 条
[1]   Indomethacin in Pregnancy: Applications and Safety [J].
Abou-Ghannam, Gael ;
Usta, Ihab M. ;
Nassar, Anwar H. .
AMERICAN JOURNAL OF PERINATOLOGY, 2012, 29 (03) :175-186
[2]  
Brandenburg K., 2012, DIAMOND
[3]  
Bruker, 2013, APEX2 SAINT SADABS
[4]   WinGX and ORTEP for Windows: an update [J].
Farrugia, Louis J. .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2012, 45 :849-854
[5]  
McIntyre JOB, 2001, PAEDIAT PERINAT DRUG, V4, P85
[6]  
Mohamed S.K., 2012, J CHEM PHARM RES, V4, P3505
[7]   THE PROBLEM OF LOW-BIRTH-WEIGHT [J].
PANETH, NS .
FUTURE OF CHILDREN, 1995, 5 (01) :19-34
[8]   A short history of SHELX [J].
Sheldrick, George M. .
ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122
[9]   Structure validation in chemical crystallography [J].
Spek, Anthony L. .
ACTA CRYSTALLOGRAPHICA SECTION D-STRUCTURAL BIOLOGY, 2009, 65 :148-155