THE SYNTHESIS AND CRYSTAL-STRUCTURE OF 1,2,3-TRI(PHENYLPHOSPHANO)[3]FERROCENOPHANE

被引：7

作者：

OSBORNE, AG ^{[1
]}

PAIN, HM ^{[1
]}

HURSTHOUSE, MB ^{[1
]}

MAZID, MA ^{[1
]}

机构：

[1] UNIV WALES COLL CARDIFF,COLL CARDIFF,SCH CHEM & APPL CHEM,CARDIFF CF1 3TB,WALES

来源：

JOURNAL OF ORGANOMETALLIC CHEMISTRY | 1993年 / 453卷 / 01期

关键词：

D O I：

10.1016/0022-328X(93)80335-9

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

1,2,3-Tri(phenylphosphano)[3]ferrocenophane has been prepared by the reaction of 1,1'-dibromoferrocene with LiP(Ph)-P(Ph)-P(Ph)Li, and its crystal structure determined by X-ray diffraction methods. The P-P bond lengths are 2,231(3) and 2.229(3) angstrom and the P-P-P bond angle is 93.5(2)-degrees. The cyclopentadienyl rings are inclined at an angle of 3.43-degrees to each other and the pseudo six-membered ring, C(1)C(6)FeP(1)P(2)P(3), is in a chair conformation.

引用

页码：117 / 120

页数：4

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