ONLINE SOLID-PHASE EXTRACTION-CAPILLARY GAS-CHROMATOGRAPHY FOR WATER ANALYSIS

被引：0
作者：
BRINKMAN, UAT
HANKEMEIER, T
VREULS, JJ
机构：
来源：
CHEMIA ANALITYCZNA | 1995年 / 40卷 / 04期
关键词：
SOLID-PHASE EXTRACTION; GAS CHROMATOGRAPHY; WATER ANALYZER; AQUEOUS SAMPLES;
D O I：
暂无
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
Solid-phase extraction (SPE) is increasingly being used to pretreat aqueous samples prior to on-line gas chromatographic (GC) analysis. The present review discusses the main problems encountered when combining 'aqueous' and 'gaseous' modules within one instrumental set-up. Next, the potential of on-line SPE-GC for the trace-level determination and identification of micropollutants in tap and surface water is demonstrated. Today, modest sample volumes (1-10 ml) suffice to obtain 0.01-0.1 mu g l(-1) detection limits for a variety of compounds if, e.g., a thermionic, flame photometric or mass-selective detector is used.
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页码：495 / 509
页数：15
相关论文
共 34 条
[1]   SOLID-PHASE MICROEXTRACTION WITH THERMAL-DESORPTION USING FUSED-SILICA OPTICAL FIBERS [J].
ARTHUR, CL ;
PAWLISZYN, J .
ANALYTICAL CHEMISTRY, 1990, 62 (19) :2145-2148
[2]   AUTOMATION AND OPTIMIZATION OF SOLID-PHASE MICROEXTRACTION [J].
ARTHUR, CL ;
KILLAM, LM ;
BUCHHOLZ, KD ;
PAWLISZYN, J ;
BERG, JR .
ANALYTICAL CHEMISTRY, 1992, 64 (17) :1960-1966
[3]   DETERMINATION OF LOW PARTS PER BILLION LEVELS OF AMINES IN URINE BY LIQUID MEMBRANE SAMPLE CLEANUP DIRECTLY COUPLED TO A GAS-LIQUID CHROMATOGRAPH [J].
AUDUNSSON, G .
ANALYTICAL CHEMISTRY, 1988, 60 (13) :1340-1347
[4]   AUTOMATIC-DETERMINATION OF N-METHYLCARBAMATE PESTICIDES BY USING A LIQUID LIQUID EXTRACTOR DERIVATIZATION MODULE COUPLED ONLINE TO A GAS-CHROMATOGRAPH EQUIPPED WITH A FLAME IONIZATION DETECTOR [J].
BALLESTEROS, E ;
GALLEGO, M ;
VALCARCEL, M .
JOURNAL OF CHROMATOGRAPHY, 1993, 633 (1-2) :169-176
[5]   LIQUID-CHROMATOGRAPHIC DETERMINATION OF POLAR POLLUTANTS IN SURFACE-WATER USING MEMBRANE EXTRACTION DISKS FOR ONLINE TRACE ENRICHMENT [J].
BROUWER, ER ;
VANIPEREN, DJ ;
LISKA, I ;
LINGEMAN, H ;
BRINKMAN, UAT .
INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY, 1992, 47 (04) :257-266
[6]  
BULTERMAN AJ, 1993, HRC-J HIGH RES CHROM, V16, P397, DOI 10.1002/jhrc.1240160703
[7]  
Cortes H.J., 1989, J MICROCOLUMN SEP, V1, P28
[8]   DIRECT INTRODUCTION OF LARGE-VOLUME URINE SAMPLES INTO AN ONLINE IMMUNOAFFINITY SAMPLE PRETREATMENT CAPILLARY GAS-CHROMATOGRAPHY SYSTEM [J].
FARJAM, A ;
VREULS, JJ ;
CUPPEN, WJGM ;
BRINKMAN, UAT ;
DEJONG, GJ .
ANALYTICAL CHEMISTRY, 1991, 63 (21) :2481-2487
[9]   REVERSED-PHASE LIQUID-CHROMATOGRAPHY COUPLED ONLINE WITH CAPILLARY GAS-CHROMATOGRAPHY .2. USE OF A SOLVENT VAPOR EXIT TO INCREASE INTRODUCTION VOLUMES AND INTRODUCTION RATES INTO THE GAS-CHROMATOGRAPH [J].
GOOSENS, EC ;
DEJONG, D ;
DEJONG, GJ ;
BRINKMAN, UAT .
JOURNAL OF MICROCOLUMN SEPARATIONS, 1994, 6 (03) :207-215
[10]  
GOOSENS EC, 1992, HRC-J HIGH RES CHROM, V15, P242
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