Synthesis of Cu Doped NiO Nanoparticles by Chemical Method

被引:48
作者
Aliahmada, M. [1 ]
Rahdar, A. [2 ]
Azizi, Y. [1 ]
机构
[1] Univ Sistan & Baluchestan, Dept Phys, Fac Sci, Zahedan, Iran
[2] Univ Zabol, Dept Phys, Fac Sci, Zabol, Iran
关键词
Precipitation method; NiO:Cu; Nanoparticles; Hysteresis loop; VSM;
D O I
10.7508/jns.2014.02.003
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
The Cu doped NiO (NiO: Cu) nanoparticles were synthesized by co-precipitation method using NiCl2.6H(2)O, CuCl2.2H(2)O for Ni and Cu sources, respectively. Sodium hydroxide has been used as a precipitator agent. Effect of Cu doping agent on the structural and optical properties of nanostructures were characterized by XRD, SEM, AFM, spectrophotometry, FTIR and VSM techniques. XRD revealed that NiO: Cu has a FCC structure. Optical absorption spectra of the samples obtained using UV-Vis spectrophotometer shows a blue-shift when copper amount increase which indicates decreasing particle size. The study of magnetization property at room temperature shows weak ferromagnetic behavior of NiO: Cu nanoparticles. Hysteresis loops were show that magnetization increasing with Cu doping up to 13% and then with further doping decreasing. (C) 2014 JNS All rights reserved
引用
收藏
页码:145 / 152
页数:8
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