SOLID-PHASE EXTRACTION AND LIQUID-CHROMATOGRAPHY ANALYSIS OF NITROFURAN COMPOUNDS IN MEAT

被引：0

作者：

POSYNIAK, A

SEMENIUK, S

NIEDZIELSKA, J

ZMUDZKI, J

机构：

来源：

CHEMIA ANALITYCZNA | 1994年 / 39卷 / 03期

关键词：

DRUG RESIDUES; NITROFURANS; SOLID PHASE EXTRACTION; LIQUID CHROMATOGRAPHY;

D O I：

暂无

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Nitrofurans were extracted from animal tissues with acetonitrile and clean-up by solid phase extraction (SPE) procedure. For dean-up C18 columns were used and retained drugs were eluted with acetonitrile containing 0.1 %(V/V) ammonia. The liquid chromatography (LC) separation was carried out on a C18 analytical column using acetate buffer and acetonitrile as the mobile phase and a UV-VIS detector. Recoveries from spiked muscles were above 80 %, and detection limit was 2 ng g-1 of tissue.

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页码：289 / 294

页数：6

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