REVERSE-PHASE LIQUID-CHROMATOGRAPHY OF P-TERT-BUTYLCALIXARENES

被引：0

作者：

VOCANSON, F ^{[1
]}

LAMARTINE, R ^{[1
]}

DUCHAMP, C ^{[1
]}

DEVAINS, JBR ^{[1
]}

机构：

[1] UNIV LYON 1,CHIM IND LAB,F-69622 VILLEURBANNE,FRANCE

来源：

CHROMATOGRAPHIA | 1995年 / 41卷 / 3-4期

关键词：

COLUMN LIQUID CHROMATOGRAPHY; P-TERT-BUTYLCALIXARENES;

D O I：

暂无

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

The p-tert-butylcalix[n] arenes (n = 4,6,7,8) and p-tert-butyldihomooxacalix[4]arene have been separated by reverse phase liquid chromatography. Optimum conditions have been obtained on a Spherisorb ODS1, 5 mu m C18 column by isocratic ambient elution with acetonitrile-methyl tert-butyl ether. Calibration plots have been obtained from purified calixarenes and the reliability of the method is confirmed from test mixtures of calixarenes of known composition.

引用

页码：204 / 206

页数：3

共 12 条

[1]

Gutsche C. D., 1989, MONOGRAPHS SUPRAMOLE

[2]

Gutsche C.D., 1989, ORG SYNTH, V68, P234

[3]

GUTSCHE CD, 1989, ORG SYNTH, V68, P238

[4] REVERSED-PHASE LIQUID-CHROMATOGRAPHIC SEPARATION OF PARA-TERT-BUTYLPHENOL-FORMALDEHYDE LINEAR AND CYCLIC OLIGOMERS [J].