ALKYLATION AND HYDROLYSIS OF PHENYLACETONITRILES UNDER MICROWAVE IRRADIATION

被引：9

作者：

BARBRY, D ^{[1
]}

PASQUIER, C ^{[1
]}

FAVEN, C ^{[1
]}

机构：

[1] UNIV SCI & TECHNOL LILLE, CHIM ORGAN & ENVIRONM LAB, BATIMENT C4, F-59655 VILLENEUVE DASCQ, FRANCE

来源：

SYNTHETIC COMMUNICATIONS | 1995年 / 25卷 / 19期

关键词：

D O I：

10.1080/00397919508011433

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Alkylation of phenylacetonitriles is performed by solid-liquid phase transfer catalysis in 1-3 minutes under microwave irradiation (one hour with a two-phase system). These nitriles can be quickly hydrolysed in a microwave oven to yield the corresponding amides or acids according to the reaction time.

引用

页码：3007 / 3013

页数：7

共 11 条

[1] C-ALKYLATION OF ACTIVE METHYLENE COMPOUNDS BY MEANS OF ALCOHOLS .7. SYNTHESIS OF ALPHA-SUBSTITUTED PHENYLACETONITRILES FROM ALPHA-PHENYLACETOACETONITRILE [J].