DETERMINATION OF 2-NITROPHENOL, 4-NITROPHENOL, 2-METHOXY-5-NITROPHENOL, AND 2,4-DINITROPHENOL BY DIFFERENTIAL-PULSE VOLTAMMETRY AND ADSORPTIVE STRIPPING VOLTAMMETRY

被引：57

作者：

BAREK, J ^{[1
]}

EBERTOVA, H ^{[1
]}

MEJSTRIK, V ^{[1
]}

ZIMA, J ^{[1
]}

机构：

[1] RES INST ORGAN SYNTH,CTR ENVIRONM & ANALYT CHEM & TOXICOL,CS-53218 PARDUBICE,CZECH REPUBLIC

来源：

COLLECTION OF CZECHOSLOVAK CHEMICAL COMMUNICATIONS | 1994年 / 59卷 / 08期

关键词：

D O I：

10.1135/cccc19941761

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The behaviour of the title substances, which are components of the commercial plant growth stimulator Sviton, in differential pulse voltammetry at a hanging mercury drop electrode was studied and the optimum conditions were established for their quantitation over the concentration region of 1 .10(-7) to 1 . 10(-5) mol 1(-1). Additional decrease in the limit of determination was achieved in adsorptive stripping voltammetry, by which 4-nitrophenol and 2-nitrophenol can be determined within the concentration regions of 2. 10(-10) to 1. 10(-7) and 2. 10(-8) to 1. 10(-7) mol 1(-1), respectively, and 2,4-dinitrophenol and 2-methoxy-5-nitrophenol within the region of 2. 10(-9) to 1. 10(-7) mol 1(-1).

引用

页码：1761 / 1771

页数：11

共 48 条

[1]

ALACRON P, 1987, CHROMATOGRAPHIA, V24, P613

[2]

BAREK J, UNPUB

[3] NONAQUEOUS ION-EXCHANGE SEPARATION TECHNIQUE FOR USE IN BIOASSAY-DIRECTED FRACTIONATION OF COMPLEX-MIXTURES - APPLICATION TO WOOD SMOKE PARTICLE EXTRACTS [J].

BELL, DA ;

KARAM, H ;

KAMENS, RM .

ENVIRONMENTAL SCIENCE & TECHNOLOGY, 1990, 24 (08) :1261-1264

[4] POLAROGRAPHIC-DETERMINATION OF SOME NITRO GROUP-CONTAINING PESTICIDES [J].

BENADIKOVA, H ;

POPL, M ;

JAKUBICKOVA, V .

COLLECTION OF CZECHOSLOVAK CHEMICAL COMMUNICATIONS, 1983, 48 (09) :2636-2643

[5]

BEYERMANN K, 1984, ORGANIC TRACE ANAL, P42

[6] HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC DETERMINATION OF 4-NITROSOPHENOLS AND 4-NITROPHENOLS IN THE PRESENCE OF PHENOL AND ALKYLPHENOLS [J].

BORYS, A .

JOURNAL OF CHROMATOGRAPHY, 1981, 216 (OCT) :361-366

[7] THE USE OF AN ALPHA-CYCLODEXTRIN MOBILE PHASE IN THE THIN-LAYER CHROMATOGRAPHIC-SEPARATION OF ORTHO-SUBSTITUTED, META-SUBSTITUTED, AND PARA-SUBSTITUTED PHENOLS [J].

BURKERT, WG ;

OWENSBY, CN ;

HINZE, WL .

JOURNAL OF LIQUID CHROMATOGRAPHY, 1981, 4 (06) :1065-1085

[8]

CHANDRA K, 1981, INDIAN J CHEM A, V20, P576

[9] COMBINATION OF TLC, GLC (OV1 AND OV17) AND HPLC (RP18) FOR A RAPID DETECTION OF DRUGS AND RELATED-COMPOUNDS [J].

DALDRUP, T ;

SUSANTO, F ;

MICHALKE, P .

FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 1981, 308 (05) :413-427

[10]

FARRAN A, 1990, ANAL CHIM ACTA, V231, P119

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