N-[(E)-4-Fluorobenzylidene]-3,4-di-methylaniline

被引:2
作者
Jin, Yue-Bao [1 ]
Chang, Yong-Kang [1 ]
Zhang, Ying [1 ]
Lei, Ke-Wei [1 ]
机构
[1] Ningbo Univ, Fac Mat Sci & Chem Engn, Inst Solid Mat Chem, State Key Lab Base Novel Funct Mat & Preparat Sci, Ningbo 315211, Zhejiang, Peoples R China
来源
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷
关键词
data-to-parameter ratio = 11.4; mean σ(C-C) = 0.003 Å; R factor = 0.040; single-crystal X-ray study; T = 293 K; wR factor = 0.103;
D O I
10.1107/S1600536812030474
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title Schiff base, C15H14FN, the N = C bond length of 1.263 (2) angstrom is shorter than the N-C bond [1.426 (2) angstrom], indicating a typical imine double bond. Moreover, the C-N-C angle is 118.5 (2)degrees. The benzene rings form a dihedral angle of 51.22 (5)degrees.
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页数:5
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共 9 条
  • [1] Non-interpenetrated square-grid coordination polymers synthesized using an extremely long N,N-type ligand
    Chen, CL
    Goforth, AM
    Smith, MD
    Su, CY
    zur Loye, HC
    [J]. INORGANIC CHEMISTRY, 2005, 44 (24) : 8762 - 8769
  • [2] DEBARBARIN COR, 1994, INORG CHIM ACTA, V219, P205
  • [3] 2-PHENYLIMINOMETHYLPHENOLS, 2-PHENYLAMINOMETHYLPHENOLS AND THEIR COPPER(II) COMPLEXES
    HARRIES, HJ
    ORFORD, BF
    BURGESS, J
    [J]. INORGANICA CHIMICA ACTA-ARTICLES, 1983, 68 (JAN): : 41 - 43
  • [4] Higashi, 1995, ABSCOR PROGRAM ABSOR
  • [5] Lindeman S. V., 1981, ACTA CRYSTALLOGR A, V37, pC87
  • [6] *RIG CORP, 1998, RAPID AUTO
  • [7] *RIG MSC, 2004, CRYSTALSTRUCTURE
  • [8] A short history of SHELX
    Sheldrick, George M.
    [J]. ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 : 112 - 122
  • [9] 2,4-Dibromo-6-{(E)-[(R)-1-phenylethyl]iminomethyl}phenol
    Xia, Dong-Guo
    Ye, Ya-Fen
    Lei, Ke-Wei
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O3168 - U1258