CRYSTAL-STRUCTURE OF (4R,5R)-2-ETHOXY-4,5-BIS[(1-METHOXY-1-PHENYL)BENZYL]-1,3-DIOXOLANE

被引：0

作者：

FENEAUDUPONT, J ^{[1
]}

DECLERCQ, JP ^{[1
]}

PATINY, L ^{[1
]}

机构：

[1] UNIV CATHOLIQUE LOUVAIN,CHIM ORGAN LAB,B-1348 LOUVAIN,BELGIUM

来源：

BULLETIN DES SOCIETES CHIMIQUES BELGES | 1995年 / 104卷 / 10期

关键词：

D O I：

暂无

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

C66H68O10, M(r) = 1021.2, orthorhombic, P2(1)2(1)2(1), a = 11.038(4), b = 14.183(6), c = 18.358(7)Angstrom, V = 2874(2)Angstrom(3), Z = 2, D-x = 1.18g.cm(-3), MoK alpha radiation (lambda = 0.71069 Angstrom). The final R indice is 0.080 for 1033 observed reflections

引用

页码：623 / 624

页数：2

共 7 条

[1] NOVEL ENANTIOSELECTIVE ACYLATING AGENTS - THE REACTIONS OF CHIRAL ORTHO ESTERS AND SILYLENOL ETHERS AS A ROUTE TO OPTICALLY-ACTIVE MONOPROTECTED 1,3-DICARBONYL COMPOUNDS [J].

BASILE, T ;

LONGOBARDO, L ;

TAGLIAVINI, E ;

TROMBINI, C ;

UMANIRONCHI, A .

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1990, (10) :759-760

[2] ENANTIOSELECTIVE ACYLATION OF ENOLATES - THE REACTION OF (4R)-TRANS-DIETHYL 2-ALKYL-2-METHOXY-1,3-DIOXOLANE-4,5-DICARBOXYLATES WITH E-SILYL AND Z-SILYL ENOL ETHERS [J].

BASILE, T ;

LONGOBARDO, L ;

TAGLIAVINI, E ;

TROMBINI, C ;

UMANIRONCHI, A .

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1991, (06) :391-392

[3] CHIRAL ORTHOESTERS IN ORGANIC-SYNTHESIS - NOVEL REAGENTS FOR THE ENANTIOSELECTIVE ACYLATION OF SILYLENOLETHERS [J].

LONGOBARDO, L ;

MOBBILI, G ;

TAGLIAVINI, E ;

TROMBINI, C ;

UMANIRONCHI, A .

TETRAHEDRON, 1992, 48 (07) :1299-1316

[4]

LONGOBARDO L, 1992, TETRAHEDRON LETT, P3421

[5]

MOTHERWELL WDS, 1978, PLUTO PROGRAM PLOTTI

[6]

Sheldrick G. M., 1985, SHELXS86 PROGRAM SOL

[7]

SHELDRICK GM, 1993, SHELXL93 PROGRAM CRY

← 1 →